Optical Microscope

16 cases · 172 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Tempered Martensite Standard: UNS clear all

Optical Microscope — sub-branches

As polished micrography 19Eletrolytically Etched Micrography by OM 6Kalling Etched Micrography by OM 34Micrography by OM 3Nital Etched Micrography by OM 110

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Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Longitudinal section micrography in a position of the thread, far from the failure. The stud presented a quenching and tempering structure and the thread was machined.
84
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the weld metal with islands of a coarse ferritic structure, degradated (recristalized) from an acicular morphology during to the long heat treatment cycle in high temperature. The post welding heat treatment (PWHT) was conducted during 12 hours at 640°C.
700
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrography of the longitudinal section of the stud presenting a tempered martensite structure, slightly banded. Hardness 45 HRc.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the longitudinal section of the bolt showing a martensitic structure, with segregation bands evidenced by the chemical etch.
99
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a transverse section of the ring presenting a uniform tempered martensite structure.
43
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The structure of the layer that is 0.7 mm thick, presented entrapped pores and globular oxides. The layer was melted after application by thermal spray (in this case using a flame) and the pin was quenched and tempered after the full application and melting of the layer.
360
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Transverse Section
Micrography of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite. The tempering was in low temperature since the hardness is high (58 HRc at the surface).
87
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Uniform Structure

More from these cases

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrography of a stud longitudinal section in the first thread fillet adjacent to the fracture, presenting a large secondary crack without any deformation evidence. This reveals a brittle material behavior, although the hardness measured at the stud end revealed 33HRc, as should be expected by the material specification.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks

+17 more from this case →

ML00129 — Non qualified WPS for High Strength SteelM - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite structure in the columnar (previous austenitic) grains has suffered degradation due to the long heat treatment cycle (12 hours) in high temperature.
96
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the weld metal, at the face, presenting regions of large ferritic grains. The acicular ferrite has suffered degradation due to the long heat treatment cycle (12 hours) in a temperature of 640°C, that is higher than the recommended for the D2 filler metal.
78
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrography of the base metal, in low magnification, showing regions of segregations in a quenched and tempered martensitic structure.
52
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the base metal showing a quenched and tempered martensitic structure. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
59
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the base metal structure, quenched and tempered martensite. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
51
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite

+12 more from this case →

ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the stud presenting a tempered martensite structure in the center of the thickness.
32
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrographic image of the stud thread, in the longitudinal section, showing the segregation lines of the steel cut at the thread indicating it was machined.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the stud at the thread bottom.
27
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the thread top, showing that the thread was machined.
29
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrography of the longitudinal section of the stud showing internal cracks, secondary (not the cracks that opened the fracture). It is evident that the cracking from the thread fillet, of a ductile aspect, presented a different aspect than the internal cracks, of a brittle aspect.
31
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Cracks

+4 more from this case →

ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the bolt at the bottom of the thread fillet, showing the uniform martensitic structure, not strain hardened.
90
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrography of the longitudinal section of the bolt at the top of the thread fillet, showing a small circunferential cracking typically of a rolling process to manufacture the thread. The thread presented no evidences of plastic deformation suggesting that the heat treatment was applied later. It is important to mention that this cracking presented no influence in the fracture of the bolt.
101
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Rolled Thread
Micrography of the longitudinal section of the bolt at the bottom of the thread fillet, in the "as polished" condition, showing the zinc flakes coating layer, applied by a painting process that do not create metallurgical bonding with the substrate.
82
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Coating Layer
Micrographic detail of the zinc flakes coating layer in the "as polished" condition of a longitudinal section of the bolt.
71
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Coating Layer
Micrography of the longitudinal section of the bolt in the center of the thickness (ND 5/8") showing a uniform martensitic structure.
67
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite

+5 more from this case →

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Micrography of a transverse section of the ring, at the pitting position, as polished, showing that there are intergranular cracks and the martensitic structure is corroded (chemical dissolution) inside the pitting.
33
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Corrosion
Micrographic detail of a transverse section of the ring, showing the corroded martensitic structure (chemical dissolution) inside the pitting.
32
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Corrosion
Micrographic detail of a transverse section of the ring, showing the corroded martensitic structure (chemical dissolution) inside the pitting.
33
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - As polished micrographyDf - Intergranular Cracking
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface.
27
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack

+4 more from this case →

ML00109 — Thermal Spray and Fuse Layer in Forged PinM - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Micrography, as polished, of the transverse section of the forged pin with the layer applied by a (thermal) spray and fuse process. The layer was melted after thermal spray application and the layer presents a continuous matrix, but there are globular oxides and pores entrapped.
29
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Surface Layer
Micrographic detail, as polished, of the transverse section of the forged pin at the interface between the pin and the spray and fuse layer. The pin was heat treated after the thermal spray, and fuse treatment. The interface presents a higher concentration of globular oxides and pores, entrapped.
23
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - As polished micrographyDf - Surface Layer
Low magnification micrography of the interface between the pin and the spray and fuse layer. Close to the surface, under the layer, the pin presents a quenched and tempered structure, compatible with a high strenght requirement. Transverse section.
20
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Surface Layer
Micrography of the pin close to the interface with the spray and fuse layer. Transverse section. The fuse is conducted in high temperature and the pin was quenched and tempered after the thermal spray deposition and fuse by flame (in this case the melting of the applied layer was conducted by a oxifuel flame.
21
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensite structure close to the interface with the spray and fuse layer. Transverse section. The fuse is conducted in high temperature and the pin was heat treated after the thermal spray deposition and fuse.
16
VIEW
ML00109 / Jan.2018
Thermal Spray and Fuse Layer in Forged Pin
M - Low Alloy Medium Carbon QTP - Tubular ForgingAp - O&G Well DrillingCd - Thermal spray
Cm - Nital Etched Micrography by OMDf - Martensite

+3 more from this case →

ML00084 — Walrus Tool SteelM - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Micrographic detail of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite, with small secondary carbides. The hardness in the section is 59 HRc.
73
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Martensite