Optical Microscope

34 cases · 338 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Tempered Martensite clear all

Optical Microscope — sub-branches

As polished micrography 41Eletrolytically Etched Micrography by OM 6Kalling Etched Micrography by OM 46Micro by OM, picric acid+FeCl3+H2O etch 3Micrography by OM 10Nital Etched Micrography by OM 232

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Multiple intergranular cracks transverse to the bolt axis. Hydrogen assisted cracking due to cathodic protection of a high strenght steel. Micrography in the "as polished" condition.
472
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Intergranular Cracking
Micrography of the welded joint fusion line presenting the liquation cracking. The weld metal is in the right side (bottom) and the forged connector heat affected zone is in the left side (top).
83
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracking
The microstructure of the pipe, presented in a longitudinal section, is an uniform tempered martensite.
105
VIEW
ML00068 / Sep.2020
Corrosion Fatigue of a 5" Drill Pipe
M - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the base metal presenting a banded microstructure in the longitudinal section of the pipe.
51
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Base metal micrographic detail presenting a tempered martensitic microstructure.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Micrographic aspect of the corrosion damage in a section transverse to the pitting.
167
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Pitting
Tempered martensitic structure of the plate base metal.
93
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
13Cr SS longitudinal section micrography, at the collapsed region, showing a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
437
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section

More from these cases

ML00073 — Hydrogen Cracking of a LAS Subsea FastenerM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Tempered martensitic structure of a longitudinal section of the fastener. Slightly banded material. Hardness level about 42 HRc.
59
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the fastener, at the threat fillet, showing a transverse cracking.
68
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Cracking
Micrography of the secondary crack, in the fillet adjacent to the nut position, where it was opened to the surface.
65
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Cracking
Micrographic detail of the secondary crack, in the fillet adjacent to the nut position, where it was opened to the surface.
46
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Cracking
Thin intergranular cracks in the center of the bolt thickness. Not continuous and not opened to the surface.
46
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking

+1 more from this case →

ML00072 — Liquation Cracks in a High Strength JointM - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
The liquation crack is a hot crack in the base metal (at the HAZ) that induces a solidification crack in the weld metal.
66
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal
Micrographic detail of the cracks at the fusion line of the welded joint, at the connector side. The cracking presents morphology of melting regions of impurities at grain boundaries of the large grains of the heat affected zone (HAZ).
57
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
The HAZ presents microcracks at previous austenite grain boundaries. These regions melted during welding and generated cracks associated to low melting temperature phases.
48
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Microcracks
The HAZ presents microcracks at previous austenite grain boundaries. These regions melted during welding and generated cracks associated to low melting temperature phases.
43
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Microcracks
Micrography of the AISI 4130 forging, 5/8" thickness, close to the welded region, in the longitudinal section.
42
VIEW
ML00072 / Jan.2018
Liquation Cracks in a High Strength Joint
M - Low Alloy Medium Carbon QTP - Longitudinal Seam Welded PipeAp - O&G Well DrillingCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal Left Side

+7 more from this case →

ML00068 — Corrosion Fatigue of a 5" Drill PipeM - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
The micrography in the as polished condition of the longitudinal section of the pipe close to the washout, shows that at the tool mark tip (notch from the external surface) a fatigue crack already started from a corroded region (pitting).
187
VIEW
ML00068 / Sep.2020
Corrosion Fatigue of a 5" Drill Pipe
M - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Micrography by OMDf - Pitting
Micrographic detail, in the as polished condition, of the corrosion fatigue crack.
89
VIEW
ML00068 / Sep.2020
Corrosion Fatigue of a 5" Drill Pipe
M - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Micrography by OMDf - Fatigue Crack
The micrography of one of the (multiple) cracks shows the slightly irregular morphology of the cracking, typical of a corrosion-fatigue mechanism.
281
VIEW
ML00068 / Sep.2020
Corrosion Fatigue of a 5" Drill Pipe
M - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
Micrographic detail of the slightly irregular crack propagation, typical of a corrosion-fatigue mechanism.
76
VIEW
ML00068 / Sep.2020
Corrosion Fatigue of a 5" Drill Pipe
M - Low Alloy Medium Carbon QTP - Seamless PipeAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Corrosion Cracking
ML00066 — GMAW Welded Joint in 9%Ni Alloy SteelM - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Micrographic detail of a longitudinal section of the base metal presenting a quenched and tempered microstructure.
49
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the low temperature heat affected zone of the pipe. The intercritical temperature (IC) is evident in the decorated grain boundaries of the previous austenite.
42
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrography of the fusion line close to the cap pass (CP). The weld metal (non etched) is in the left side.
43
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line
Micrography of the heat affected zone, a little far from the fusion line, close to the base metal.
40
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the fusion line in the center of the thickness, where the heat affected zone was reheated by the subsequent passes.
34
VIEW
ML00066 / May.2017
GMAW Welded Joint in 9%Ni Alloy Steel
M - Nickel Alloy SteelP - Welded Testpiece for QualificationAp - PipelineCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line

+8 more from this case →

ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the heat-affected zone close to the base metal.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the heat-affected zone close to the fusion line.
31
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the tempered martesite weld metal close to the fusion line. The columnar grains can be observed .
22
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Weld Metal
Micrography of the base metal showing a tempered martensitic microstructure.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Micrography of the heat-affected zone. The fusion line is in the right and the coarse structure of the base metal is refined at the heat affected zone.
28
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone

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ML00010 — Cold Cracks in a Gouged Weld MetalM - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Detail of the tempered martensitic structure of the plate base metal. Hardness level of 27 HRc.
92
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of a transverse section of the weld at the heat affected zone region. The macrosection was hardness tested and the base metal hardness is 27HRc, the HAZ is 32HRc and the weld metal is 45HRc, revealing something wrong in the weld metal at the position close to the cracked area.
79
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Transverse Section
High temperature heat affected zone of the plate, welded in repair. The micrography was taken from a sample collected close to the cracked region, but not containing any macroscopic cracking.
76
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Detail of the high temperature heat affected zone of the plate, welded in repair.
69
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
The weld metal, hard, presented a martensitic structure, probably due to the localized increase in carbon content, from the unsuitable carbon arc gouging procedure.
63
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

+5 more from this case →

ML00039 — Collapse in Tubular 13CrM - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
13Cr SS in the longitudinal section, at the collapsed region. Non uniform structure (ferritic matrix and decorated prior austenite grain boundaries) that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
54
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
13Cr SS in the longitudinal section, at the collapsed region. Detail of the non uniform structure (ferritic matrix and decorated prior austenite grain boundaries) that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
48
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Prior Austenite Boundaries Decorated
13Cr SS in the transverse section, at the collapsed region, showing a non uniform structure that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
29
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Transverse Section
13Cr SS transverse section micrography, at the collapsed region, showing a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
29
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Transverse Section
The micrography of the 13Cr SS in the transverse section, at the collapsed region, shows a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
32
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Overtempered Structure

+3 more from this case →