Optical Microscope

162 cases · 600 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Detail focus: Microstructure clear all

Optical Microscope — sub-branches

As polished micrography 13Chromic Acid Electrolytic Etched 4Eletrolytically Etched Micrography by OM 4FeCl3+HCl+Ethanol Etched Micro 6FeCl3+HCl+H2O Etched Micro 17Glyceregia Etched Micrography by OM 5H2SO4+HNO3+H3PO4 Etched Micro 2Kalling Etched Micrography by OM 62Keller Etched Micrography by OM 7Kroll Etched Micrography by OM 3Micro by OM, HCl + Ethanol + Picric Acid 6Micrography by OM 17Micrography by OM using A262 Method A 39Micrography by OM, HF + HNO3 + H2O etch 6NH4OH+H2O+H2O2 Etched Micro 3NaOH Electrolytic Etched Micro 44Nital Etched Micrography by OM 329Oxalic Acid Electrolytic Etch 33

Results

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Micrography of a longitudinal section of the housing presenting a uniform tempered martensitic structure. The material presented a thickness about 2.5 mm in the region where the cracking started.
52
VIEW
ML00093 / Sep.2017
MIC of a Drilling Tool
M - Low Alloy Medium Carbon QTP - Heat Treated PartAp - O&G Well DrillingCd - Brittle Behavior
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrographic aspect of the disc in the longitudinal section. Tempered martensitic structure, probably strain hardened.
30
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the longitudinal section of the pin showing a tempered martensite structure, with bands that are associated to segregations. The pin presented average hardness of 38 HRc in the section.
63
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the transverse section of the rail, in the head, showing a fully perlitic structure.
374
VIEW
ML00091 / Sep.2017
Flat Bottom Rail TR57
M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the slightly banded perlitic structure, in the center of the thickness. ND 3". 7.6 mm thick.
530
VIEW
ML00090 / Sep.2017
Carbon Steel Tubing for Structural Application
M - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrographic detail of the bainitic structure in the center of the pin, that was quenched and tempered after carburizing.
75
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainite

More from these cases

ML00080 — MIC of Stacking Disc SpringsM - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Micrographic aspect of the disc in the transverse section. Tempered martensitic structure, probably strain hardened.
31
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Nital Etched Micrography by OMDf - Martensite
ML00009 — Hydrogen Cracking of a 5" Drill Pipe S135M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the pin showing a tempered martensite structure. The pin presented average hardness of 38 HRc in the section.
53
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the longitudinal section of the pin showing a tempered martensite structure. The pin presented average hardness of 38 HRc in the section.
55
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
ML00091 — Flat Bottom Rail TR57M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Micrographic detail of the transverse section of the rail, in the head, showing a fully perlitic structure.
42
VIEW
ML00091 / Sep.2017
Flat Bottom Rail TR57
M - High Strength Low AlloyP - RailAp - TransportationCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Perlite
ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
ML00090 — Carbon Steel Tubing for Structural ApplicationM - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Micrography of a longitudinal section of the tube, in the center of the thickness. ND 3". 7.6 mm thick.
55
VIEW
ML00090 / Sep.2017
Carbon Steel Tubing for Structural Application
M - Low Carbon SteelP - TubeAp - StructureCd - Typical manufacturing
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, close to the surface (ND 1/2"). The grain size is higher than the center of the bolt.
28
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the pin, at the surface. The pin was carburized, quenched and tempered (yellow diffuse layer at the surface, 0.5 mm of extension) and a white layer of hard chromium plating is evident.
108
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Carburized Layer
Micrographic detail of the high hardness martensitic structure at the surface of the pin, that was quenched and tempered after carburizing.
67
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography that presents a secondary cracking (adjacent to the broken surface) propagating 500 microns from the surface, where there is a white layer of hard chromium .
78
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Carburized Layer
The as polished micrography of a longitudinal section of the pin, showing several microcracks associated to the chromium layer.
56
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Hard Chromium Layer
The as polished micrography of a longitudinal section of the pin, showing that under the white layer of hard chromium (about 10 microns thick), there are already intergranular microcracks.
52
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Hard Chromium Layer