Optical Microscope

8 cases · 99 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Product: Tube Condition: Damage clear all

Optical Microscope — sub-branches

As polished micrography 16FeCl3+HCl+Ethanol Etched Micro 7FeCl3+HCl+H2O Etched Micro 7Micrography by OM using A262 Method A 7Nital Etched Micrography by OM 62

Results

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BASE METAL SURFACE - Ferritic structure, grain refined.
90
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Base Metal
Uniform granular microstructure of the aluminum brass, monophasic alpha.
44
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Alpha
Micrography of the tranverse section of the tube, in the center of the thickness. There are small grains and large grains, characterizing a dual grain size. The large grains size is about 100 microns, more than 10 times larger than the average size of the smaller grains size.
101
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Dual grain sizes
The tube microstructure is ferritic-pearlitic, typical of this kind of material. No evidences of microstrutural changes were detected (no overheating, no decarburization).
177
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the longitudinal section of the tube, close to the external surface. The carburizing layer consists of a bainitic structure, with intergranular and intragranular carbide precipitation.
1185
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Carburized Layer
The micrography of the longitudinal section of the tube, close to OD, shows the paralel cracks, filled with oxides, perpendicular to the surface.
1442
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in the colder part of the equipment, position 1. The material presented carbide precipitation at grain boundaries (not yet fully surrounding the grains) and at this point the tube presented no internal corrosion.
338
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
The micrography shows the region underbead, of the tube HAZ, responsible for the hydrogen cracking (fracture in the right side of the photo - black). The hardness of the HAZ is about 600 HV.
55
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Cracking

More from these cases

ML00177 — Cr-Mo Seam Welded TubeM - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
BASE METAL SURFACE - The micrography (transverse to the tube) presents the ferritic/pearlitic/bainitic structure.
75
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Granular structure
BASE METAL SURFACE - The microstructure of the base metal is ferritic/pearlitic/bainitic.
74
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Grain refined structure
HAZ SURFACE
72
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
HAZ SURFACE
66
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Last Bead HAZ
HAZ SURFACE
55
VIEW
ML00177 / Dec.2021
Cr-Mo Seam Welded Tube
M - CrMo SteelP - Longitudinally Seam WeldedAp - Fired HeaterCd - Not according to spec
Cm - Nital Etched Micrography by OMDf - Bainitic HAZ

+18 more from this case →

ML00170 — MIC in Aluminum Brass TubesM - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Micrographic detail of the granular structure of the aluminum brass, monophasic alpha.
44
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Alpha
Micrography of a transverse section of the tube, close to the leakage point. The thickness is localized reduced where the internal passive layer was ruptured, and the chemical effect of the biological proliferation created a high corrosion rate.
26
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Localized Thinning
Micrography of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
28
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
Micrographic detail of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
26
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
MIC in Aluminum Brass Tubes
2
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Localized Corrosion

+1 more from this case →

ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Micrographic detail of the alpha microstructure presenting dual grain sizes. Two different types of twins are presented in the structure: annealing twins and deformation twins, suggesting that the material was probably partially recristalized after cold deformation and stress relief treatment.
87
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Alpha
Micrography of a transverse section of the bent tube, external surface (OD) to the top and internal surface (ID) to the bottom of the figure. At the through wall cracking position, the external surface presented a layer of intergranular corrosion.
95
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Cracking
Micrographic detail of the external side of the bent tube, as polished, showing detachement of several grains due to the intergranular corrosion layer. The corroded layer is about 200 microns thick at this position.
89
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Intergranular Corrosion
Micrographic detail of the external side of the tube, showing the layer of intergranular corrosion and the through ewall integranular stress corrosion cracking.
88
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Through Wall Cracking
Micrography of the external side of the bent tube, showing detachement of several grains due to intergranular corrosion. The corroded layer is about 200 microns thick at this position. The differences of colours in the corroded layer suggests a dealloying effect, also known as selective leaching.
71
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - External Surface

+4 more from this case →

ML00163 — Corrosion Fatigue of a Boiler Waterwall TubeM - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
The internal side of the tube presented multiple cracks, filled with oxides, blunt-tipped, typical of a corrosion fatigue cracking mechanism.
160
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - As polished micrographyDf - Parallel cracks
Micrographic detail of the corrosion cracking from internal side of the tube, in several points at the tube surface.
156
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - As polished micrographyDf - Corrosion Cracking
Low magnification micrography of the multiple cracks, parallel, transgranular. No evidences of microstrutural changes (heat evolution or decarburization).
127
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Transgranular Cracking
Micrography presenting the internal tube surface with several parallel cracks, some still in the beginning (less than 0.1 mm deep).
115
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Parallel cracks
Micrography of the crack tip, initiated from the internal tube surface. The crack is transgranular, filled with oxides and blunt-tipped.
109
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Transgranular Cracking

+9 more from this case →

ML00107 — Carburized 9Cr1MoV Superheater TubeM - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Micrography of the longitudinal section of the tube, close to the internal surface. A thick scale is evident, but no microstructural changes compared to the center of the tube.
183
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
156
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
137
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the tube in the center of the thickness, showing a ferritic-bainitic structure of this CrMoV steel.
142
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of the longitudinal section of the tube, close to the external surface, presenting a thick deposit.
110
VIEW
ML00107 / Dec.2017
Carburized 9Cr1MoV Superheater Tube
M - Heat Resistant SteelP - Seamless tubeAp - BoilerCd - Carburization
Cm - As polished micrographyDf - Close to the External Surface

+7 more from this case →

ML00104 — Thermal Fatigue of a Boiler TubeM - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
The micrography of the longitudinal section of the tube, close to ID, shows the paralel cracks, filled with oxides, perpendicular to the surface.
229
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Close to the Internal Surface
Micrographic details of the longitudinal section of the tube, close to OD, showing paralel cracks, filled with oxides, perpendicular to the surface.
115
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Cracks Transverse to the Surface
Micrographic details of the longitudinal section of the tube, close to OD, showing paralel cracks, filled with oxides, perpendicular to the surface.
109
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Thermal Fatigue Cracks
Micrographic details of the longitudinal section of the tube, close to ID, showing paralel cracks, filled with oxides, perpendicular to the surface.
103
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Cracks Transverse to the Surface
Micrographic details of the longitudinal section of the tube, close to ID, showing paralel cracks, filled with oxides, perpendicular to the surface.
99
VIEW
ML00104 / Dec.2017
Thermal Fatigue of a Boiler Tube
M - Low Carbon SteelP - Autogenously Welded TubeAp - BoilerCd - Thermal Fatigue
Cm - As polished micrographyDf - Thermal Fatigue Cracks

+10 more from this case →

ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 2, where the temperature was higher and the carbide precipitation increased during service.
272
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrography of the 1.65 mm thickness tube, in the middle of the thickness of the longitudinal section. This part of the tube is located in position 3, where intergranular and transgranular carbide precipitation occurred during service.
234
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrographic detail of the intergranular corrosion at the internal surface of the tube in position 2. Several grains were already removed by the corrosion.
171
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 3, at the internal surface. Although there is a strong precipitation, both intergranular and transgranular, the tube did not corrode at this point.
144
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intragranular Secondary Precipitation

+1 more from this case →

ML00052 — Cold Cracks in API 5CT L80 Tube Welded to a Structural PartM - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Low carbon plate base metal presenting the ferritic perlitic structure.
55
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
High Strenght Low Alloy steel tube, base metal, presenting the bainitic structure.
54
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the low carbon steel plate at the fusion line, presenting a bainitic structure at the HAZ and ferritic structure in the weld metal.
82
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
The micrography shows the martensitic region of the tube HAZ responsible for the hydrogen cracking, presenting too high hardness level (600 HV). It is a fresh martensite since the joint was welded in one pass and there was no PWHT.
45
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the weld metal in the center of the fillet showing a 100% acicular ferrite that is a microestructure of a high strenght steel, evidenced the effect of the dilution of the tube chemistry in the weld metal.
40
VIEW
ML00052 / Apr.2017
Cold Cracks in API 5CT L80 Tube Welded to a Structural Part
M - Low Alloy SteelP - Seamless tubeAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

+1 more from this case →