Kalling Etched Micrography by OM

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
492
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
17-4 PH rod. Micrography of the longitudinal section in the center of the thickness, presenting an aged martensitic structure. The darker lines are bands of (sligthly) segregated regions. This material presents properties that correspond to the H1150 grade.
73
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
Original casting base metal presenting a coarse martensitic structure with a small amount of delta ferrite.
50
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Base metal micrographic detail presenting a tempered martensitic microstructure.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Blade microstructure. Tempered martensite, (probably) retained austenite and delta ferrite islands.
55
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Delta Ferrite Islands
Transverse section of the 1/16" thick tube at the autogenous seam weld.
588
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Autogenous Weld

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ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). The adopted filler metal is similar to the base metal.
27
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). There is a region where the primary carbides melted (partially melted zone), that appears dark, and a region of high dilution cloe to the fusion line.
26
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line

+4 more from this case →

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00121 — Pitting Corrosion in a Subsea SystemM - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
17-4 PH rod. Micrography of the longitudinal section in the center of the thickness, presenting an aged martensitic structure. The darker lines are bands of (sligthly) segregated regions. This material presents properties that correspond to the H1150 grade.
66
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
17-4 PH rod. Micrographic detail of the aged martensitic structure. At this magnification level the previous austenite grain boundaries are evidenced. It is also possible to see that the bands of (sligthly) segregated regions are all martensitic.
64
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Martensite
17-4 PH rod. Micrography of the longitudinal section close to the surface, presenting the roughness (the waves at the surface) and a region where a pitting was still in the beginning, not related to any specific microstructure.
70
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Pitting
ML00055 — CA6NM Blade Remanufactured by WeldingM - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Inserted casting base metal presenting a coarse martensitic structure with a small amount of delta ferrite.
24
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Micrography of the original casting blade at the fusion line of the welding with the insert casting. There is a refinement effect on the coarse base metal structure.
24
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Left Side
Micrographic detail of the fusion line of the original casting blade welded to the insert casting. There is a refinement effect on the coarse base metal structure.
21
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Left Side
Micrography of the inserted casting at the heat affected zone of the welding with the original casting. There is a refinement effect on the coarse base metal structure.
20
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Right Side
Micrographic detail of the fusion line of the inserted casting welded to the original casting. There is a refinement effect on the coarse base metal structure.
15
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Right Side

+2 more from this case →

ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the heat-affected zone close to the base metal.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the heat-affected zone close to the fusion line.
31
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the tempered martesite weld metal close to the fusion line. The columnar grains can be observed .
22
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Weld Metal
Micrography of the base metal showing a tempered martensitic microstructure.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Micrography of the heat-affected zone. The fusion line is in the right and the coarse structure of the base metal is refined at the heat affected zone.
28
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone

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ML00017 — Casting Defect in CA6NMM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Blade microstructure. Previous austenite coarse grains.
46
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Coarse Structure
Blade microstructure. Tempered martensite, (probably) retained austenite and delta ferrite islands.
47
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Delta Ferrite Islands
Region of a casting void in the blade.
33
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Void
Blade structure close to the region where the voids were detected.
40
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Non Metallic Inclusions
ML00026 — Autogenous Seam Welded Tube in Ferritic SSM - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
97
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
68
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Equiaxial grains of a ferritic structure, in a longitudinal section of the tube.
49
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Ferrite
Equiaxial grains of a ferritic structure, in a transverse section of the tube.
40
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Equiaxial grains of a ferritic structure, in a transverse section of the tube.
35
VIEW
ML00026 / Feb.2017
Autogenous Seam Welded Tube in Ferritic SS
M - Ferritic Stainless SteelP - Fabrication WeldAp - AutomotiveCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains

+5 more from this case →