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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Secondary carbides clear all

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Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
491
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Aspect as received, side A, of the part removed from the rectangular tube that was manufactured from plates, and originally presented two welded seams (not included in the sample). Close to the edges of the sample, where probably were the corners of the rectangular tube, the degradation is in a highest level. Three samples were analysed, with different thicknesses (indicated in the figure). Side A is the side that was in contact with the reaction (product side).
445
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Aspect of the serrated walrus tool, interchangeable, that was removed at the end of its life. Dimensions of 1" thick, 2" width, 3" long.
419
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Aspect Before AnalysisDf - General View
Micrography of the new tube close to a region of a casting defect (shrinkage), presenting only austenitic structure with a network of primary precipitates.
351
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Aspect of the rusted knife, before cleaning.
1195
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Aspect Before AnalysisDf - Corrosion
Micrography of the transverse section of the NEW TUBE, in the center of the thickness, showing the austenitic structure with primary carbides network.
410
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
The intake valve seat cylinder, manufactured in a high alloy white cast iron, presents a network of primary carbides, not degradated even after high temperature exposition during all lifetime.
632
VIEW
ML00003 / Apr.2017
Cast iron Engine Valve Seats
M - White Cast IronP - Valve SeatAp - MaritimeCd - Microstructural Evolution
Cm - Micrography by OMDf - Network of Primary Carbides

More from these cases

ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Condition of the joint between the centrifugally cast tube (bottom) and the buttered fitting (top). During this welding the cast fitting (buttered) showed several cracks but after removal of the fitting it was clear that the cracks were formed during the buttering and not during the joining.
46
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect Before AnalysisDf - General View
After removal of the cracked part of the fitting, the dye check test indicated the presence of several cracks in the internal diameter (ID), out of the buttered layer, that means, in the fitting base metal.
42
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Aspect by NDTDf - Cracks
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure

+13 more from this case →

ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Aspect as received, side B, of the same part. Side B is the external side of the rectangular tube, that was in contact with the electric furnace atmosphere. This surface of side B presented less degradation than the internal surface (side A).
88
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Aspect Before AnalysisDf - General View
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation

+22 more from this case →

ML00084 — Walrus Tool SteelM - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Micrography of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite. The tempering was in low temperature since the hardness is high (58 HRc at the surface).
87
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrographic detail of the tool steel, in the longitudinal section of the part. The material presented a uniform structure, tempered martensite, with small secondary carbides. The hardness in the section is 59 HRc.
73
VIEW
ML00084 / Mar.2020
Walrus Tool Steel
M - High Carbon Tool SteelP - ForgingAp - Mechanical IndustryCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Martensite
ML00097 — Cast SS Tube Removed From High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
The macrography of a transverse section of the new tube shows that there are shrinkage voids close to the internal surface, that is exposed to high temperature air. The tube is a 4" diameter and 1/4" thick.
62
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure
Micrography close to the external surface of a new tube, sound.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the External Surface
Micrography close to the internal surface of a new tube, presenting casting defects.
47
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the tube removed from service after 6 month, close to a region of a casting defect (shrinkage), presenting austenitic structure with a network of primary precipitates (initial stage of coarsening) and intragranular secondary precipitation.
48
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
The macrography of a transverse section of the tube removed from service after 6 months, with damage close to the internal tube surface. The tube is a 4" diameter and 1/4" thick.
41
VIEW
ML00097 / Nov.2017
Cast SS Tube Removed From High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - High Temperature
Cm - Transverse Section AspectDf - Casting Structure

+2 more from this case →

ML00054 — Cutlery CorrosionM - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Detail of the rusted surface of the knife, before cleaning.
340
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Surface AspectDf - Corrosion
Tempered martensitic microstructure of the knife observed in a transverse section micrography. There are also secondary carbides (white globules) that increase the material wear resistance.
254
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite
Detail of the tempered martensitic microstructure with secondary carbides of the knife, observed in a transverse section micrography.
206
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite
Aspect of the rusted surface after cleaning, showing adhered products at the surface, in regions where the passive layer was destroyed and pitting corrosion occurred.
184
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Corrosion
Detail of the rusted surface. EDS analysis inside the pitting shows a high Cl peak (the bright aspect inside the pitting), indicating that the salt over the surface was responsible for destroying the passive layer and the localized corrosion occurred.
172
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Corrosion

+3 more from this case →

ML00038 — Cast SS Tube for High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Micrography of the transverse section of the NEW TUBE, close to the external surface, showing the austenitic structure with primary carbides network.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface
Macrography of the NEW TUBE, centrifugally cast, in the transverse section, presenting columnar grains close to the external surface.
50
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Kalling Etched MacroDf - Transverse Section
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects close to the external surface.
49
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects in the center of the thickness.
47
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Transverse Section
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE, in the center of the thickness, showing the austenitic structure with primary carbides network and secondary precipitation.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation

+4 more from this case →

ML00003 — Cast iron Engine Valve SeatsM - White Cast IronP - Valve SeatAp - MaritimeCd - Microstructural Evolution
The intake valve seat cylinder, manufactured in a high alloy white cast iron, presents a network of primary carbides, not degradated even after high temperature exposition during all lifetime.
206
VIEW
ML00003 / Apr.2017
Cast iron Engine Valve Seats
M - White Cast IronP - Valve SeatAp - MaritimeCd - Microstructural Evolution
Cm - Micrography by OMDf - Network of Primary Carbides
The exhaust valve seat cylinder, manufactured in a high alloy white cast iron, presents a coalesced structure, degradated by high temperature exposition during the lifetime.
182
VIEW
ML00003 / Apr.2017
Cast iron Engine Valve Seats
M - White Cast IronP - Valve SeatAp - MaritimeCd - Microstructural Evolution
Cm - Micrography by OMDf - Coalesced structure
The exhaust valve seat cylinder, manufactured in a high alloy white cast iron, presents a coalesced structure, degradated by high temperature exposition during the lifetime.
137
VIEW
ML00003 / Apr.2017
Cast iron Engine Valve Seats
M - White Cast IronP - Valve SeatAp - MaritimeCd - Microstructural Evolution
Cm - Micrography by OMDf - Coalesced structure