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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Fractographic aspect of the stud fracture surface, by scanning electron microscopy, close to the bottom of the thread fillet. In the center of the image it is possible to see secondary cracks with intergranular morphology.
59
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. The deep corrosion in a short time is only possible associated to the biological growth and aggressive environment generated by the microorganisms metabolites - Microbiologically Induced Corrosion (MIC).
104
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Deposits
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a seamless pipe in a low alloy steel X70 cladded by welding overlay of Alloy 625 (by automatic GTAW process). The region is a detail of the interface inside the Ni alloy weld metal, presenting columnar grains and intragranular preciptation. The pipe was heat treated before bending (solution annealing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
656
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Fractography of the roller bearing, close to the external surface. In this position the fracture of the cylindrical roller bearing shows micromechanisms of decohesion at large carbides (cracked) and quasecleavage, typical of overloading this high strength tool steel (martensitic with carbides at 64 HRc).
75
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Close to the External Surface
Aspect of the bolt fracture surface by scanning electron microscopy, (SEM) presenting striations that indicate a FATIGUE micromechanism. The bolt is of a medium strength (class 8.8) low alloy steel, medium carbon, quenched and tempered.
1123
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Scanning electron microscopy image of the chromium plated cylinder surface, presenting deposits and localized dissolution under deposits. There are different stages of corrosion in this region, observed in low magnification. Small areas of attack and a shallow pitting with deposits that were analyzed by EDS and revealed the presence of S.
903
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Surface Aspect by SEMDf - Localized Corrosion
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranular, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
517
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fracture

More from these cases

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by scanning electron microscopy of the secondary cracks with intergranular morphology.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Secondary Cracks
Micrography of the bottom of the thread fillet, presenting secondary cracks of intergranular morphology, propagating transverse to the stud axis, but presenting longitudinal openings.
28
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by SEMDf - Cracks
ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Microscopical aspect by scanning electron microscopy (SEM) of the external surface of a drilling tool in a position that presented localized deposits and corrosion under deposit. It is possible to see that the strain hardened surface was etched by the aggressive metabolites of the microorganisms.
90
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Fractographic aspect of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
54
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
Fractographic detail of the valve body fracture surface after opening the crack. The fracture micromechanism is brittle, by cleavage, with several secondary microcracks associated to the sigma phase.
52
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets

+1 more from this case →

ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Image by scanning electron microscopy of the interface of the internally cladded pipe. It is a seamless pipe in low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process). The region is a detail in the side of the Ni alloy weld metal, presenting transgranular precipitation. The pipe was heat treated before bending (solution annelaing) and after bending (quenching and tempering to meet X70 grade). The microhardness of this region is higher than the value obtained out of this region, in the overlay.
42
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
Image by scanning electron microscopy of the interface of the internally cladded pipe, seamless low alloy steel X70 overlaid with Alloy 625 (by automatic GTAW process) and presenting maximum iron content of 5% at the thickness of 3 mm (the qualified thickness).
36
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Electrolytic Etch Micrography by SEMDf - Clad Interface
ML00131 — Brittle Failure of a Soft Roller BearingM - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Aspect of the roller bearing fracture surface, by scanning electron microscopy, close to the internal surface. In this position the fracture shows ductile micromechanisms (dimples) as well as decohesion of large carbides and (brittle) cleavage facets, typical of overloading this low strenght, and low toughness, ferritic structure (21 HRc). The structure in this region, ferritic with large broken carbides and small rounded carbides, is of a low toughness, as indicated by the fracture.
54
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Close to the Internal Surface
Fracture micromechanism at a region close to the internal surface. In this position the fracture shows ductile micromechanisms (dimples) as well as decohesion of large carbides and (brittle) cleavage facets, typical of overloading this low strenght ferritic structure (21 HRc). The structure in this region, ferritic with large broken carbides and small rounded carbides, is of a low toughness, as indicated by the fracture.
44
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Close to the Internal Surface
Fracture micromechanism at a region close to the external surface. In this position the fracture shows quasecleavage, as well as decohesion of large carbides. typical of overloading this high strenght martensitic structure (64 HRc).
44
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Close to the External Surface
ML00130 — Fatigue Fracture of Overloaded BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Aspect of the fracture surface in low magnification, showing a flat aspect (associated to a fatigue fracture micromechanims) and a rough aspect (associated to a ductile fracture micromechanism).
167
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Fractography by SEMDf - General View
Aspect of the fracture surface by scanning electron microscopy, presenting fatigue striations micromechanism. The bolt is a medium strength low alloy steel, medium carbon, quenched and tempered.
153
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Detailed fractographic aspect of the flat part of the bolt fracture, presenting fatigue striations. The bolt is a medium strength low alloy steel, medium carbon, quenched and tempered.
141
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Fractographic detailed aspect of the rough part of the fracture surface, presenting ductile dimples. This is the final fracture, by overload.
137
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Ductile Fracture
ML00128 — MIC of a Stored Hydraulic CylinderM - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Scanning electron microscopy image of the chromium plated surface in a position where the cylinder was not damaged, showing the surface finishing.
35
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Surface Aspect by SEMDf - At the Surface
Scanning electron microscopy image of the chromium plated cylinder in a region of localized dissolution under deposit. Inside the shallow pitting the Cr structure with a network of layers is revealed by the etching effect promoted by microbiollogically induced corrosion.
35
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Surface Aspect by SEMDf - Corrosion
Scanning electron microscopy image in detail of the chromium plated cylinder surface in a region of localized dissolution. The surface shows several microcracks promoted by the effects of the microbiollogically induced corrosion. Inside the corroded pit the network of the chromium layer is evidenced by the MIC attack.
48
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Surface Aspect by SEMDf - Corrosion
ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranuar, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
37
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking