High Alloy Steel

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Intragranular Intergranular Precipitates Capture method: Oxalic Acid Electrolytic Etch clear all

High Alloy Steel — sub-branches

Austenitic Stainless Steel 1

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SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag

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ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 1 AT THE FRACTURE - Micrographic detail of the intergranular fracture. The austenitic grains of the material are loosing.
80
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Fracture
SAMPLE 1 AT 1 mm THICKNESS - Micrography in low magnification in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation.
77
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 1 AT 1 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular.
76
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 1 AT 1 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides.
72
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation

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