Austenitic Stainless Steel

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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The circumferential welds presented several regions where the multiple cracks appeared, mainly revealed by dye check test.
49
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect by NDTDf - Multiple cracks
Detail of the external side of the stub end showing that the cracking is circunferential, located in a corroded surface, that corresponds to the confined region under the flange.
85
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Cracking
Low magnification fractography by scanning electron microscopy, after a complete opening of the crack. At this magnification no micromechanism is evident.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fracture
Transverse section macrography of the plate where the degradation by thinning is worst, close to the original corners of the tube. The thinning is occurrring from the product reaction side (side A to the bottom of the figure). The macrography shows a reduction in the thickness from 2 mm (right side, sample 2) to almost zero (left side, sample 1).
86
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Transverse Section AspectDf - Thinning
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
757
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Aspect of a crevice corrosion of the flange, under the bolt head, showing evidences that the cathodic protection system was not connected to the stainless steel instrument.
1434
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Aspect Before AnalysisDf - Localized Corrosion
The scanning electron microscopy image of the internal surface of the tube in position 2 shows a localized corrosion region with intergranular morphology, as well a crack from the corroded region.
1237
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrographic detail of the fatigue cracking at the margin of the flange to shell fillet weld.
485
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack

More from these cases

ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
The small sample removed for analysis. This wedge sample presents three faces: one polished face (that corresponds to the surface), one fractured face and one cut face.
38
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Testpiece aspectDf - Fracture
The small wedge sample is 4 mm deep in the thickness and the circumferential weld are is about 15 mm width where it appears in the internal side of the carcass. The image shows the crack surface (fracture) where the weld aspect is evident.
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Aspect Before AnalysisDf - Fracture
The fracture surface in the sample shows columnar grains in the weld and large facets in the heat affected zone (HAZ) close to the internal surface of the carcass (to the top of the image).
32
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture
Detail of the fracture in the heat affected zone, showing a flat fracture where the fracture is close to the surface of the plate, exposed to the high temperature exhausting gases.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Fractography by SEMDf - Brittle Fracture
Detailed microstructure of the plate base metal, exposed to high temperature exhausting gases. Refined austenite, precipitation of carbides in the grain boumdaries and some cracks.
24
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Crack

+2 more from this case →

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Macrographic detail of the longitudinal section of the stub end, showing the external side to the top and the internal side to the bottom. There are multiple cracks starting from the external side.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Longitudinal Section AspectDf - Multiple cracks
Micrography of the stub end longitudinal section, presenting multiple cracks, branched.
40
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - As polished micrographyDf - Multiple cracks
Micrography of the stub end longitudinal section, showing multiple branched transgranular cracks.
25
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transgranular Cracking
Micrography of the stub end longitudinal section, showing multiple branched transgranular cracks, typical of a Chloride Stress Corrosion Cracking mechanism.
34
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Corrosion Cracking
Micrographic details of the Chloride Stress Corrosion Cracks, transgranular and branched.
34
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Corrosion Cracking

+1 more from this case →

ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Flat aspect of the fracture. The striation micromechanism is revealed.
50
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
The thin striation is evident in the fracture surface, suggesting a high cycle fatigue, typically identified in vibration conditions.
45
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
Detail of the striation micromechanism.
48
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
When the fracture propagates, the striation becomes wider and with transgranular irregular steps.
47
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
Micrography of a longitudinal section of the flared tubing where the fracture occurred. The starting point of the fracture is associated to the external side of the tubing, where it was connected by a nut and there was a localized plastic deformation due to the fitting assembly.
33
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Transgranular Fracture

+1 more from this case →

ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Longitudinal section macrography of the plate where the degradation by thinning is reducing the thickness from 6mm to 4mm (sample 3). The thinning is occurrring from the product reaction side (side A to the bottom of the figure).
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Longitudinal Section AspectDf - Thinning
SAMPLE 1 AT THE FRACTURE - Micrographic detail of the intergranular fracture. The austenitic grains of the material are loosing.
80
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Fracture
SAMPLE 1, AT THE FRACTURE - Micrography, as polished, of the oxides at the fracture (zero thickness). In this region the oxide layer penetrated through thickness, intergranular, and fractured the material.
63
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - Intergranular Fracture
SAMPLE 1, AT THE FRACTURE - Micrographic detail, as polished, of the oxides that are penetrating in the austenitic grain boundaries. The oxidation created intergranular cracks in regions close to the edge of the rectangular tube, that are more susceptible to suffer cyclic thermal stresses, since the furnace is weekly turned off, during two days.
55
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - Intergranular Cracking
SAMPLE 1 AT THE FRACTURE - Micrographic detail by scanning electron microscopy, as polished, of the oxides that are penetrating in the grain boundaries. The EDS showed high Molibdenium content in the penetrating oxides. The process uses Mo oxides to make metallic Mo and the high Mo content at the surface could be responsible for reducing the oxidation resistance of the material and intensifying the thinning at the process side (side A).
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Micrography by SEMDf - Oxide Layer
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Aspect of a broken 5/16" bolt that was operating inside the pressure vessel in a condition that exceeds the limits of use of the AISI 316 steel. The fracture is located close to the position where there was the bolt head and the threads were "removed" close to the fracture surface.
75
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Fracture
Low magnification SEM image showing the brittle aspect of the cracks in the bolt thread.
61
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Cracks
Detail of the bolt thread in a SEM image, showing parts of the thread removed in a brittle way.
62
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Brittle Fracture
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

+2 more from this case →

ML00122 — Crevice Corrosion in a Subsea SystemM - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Detail of the electronic device after removing the external case. It is corroded because seawater entered in the equipment that was pressurized from the external sea environment.
228
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Aspect Before AnalysisDf - Corrosion
After a longitudinal cut of the case it was possible to see that a localized corrosion has occurred associated to the regions where there were sealed holes, plugged, in a crevice condition, not related to any welded position.
193
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Transverse Section AspectDf - Corrosion
Macrography of the longitudinal section of the case, that was welded to padeyes. The corrosion occurred in a region where there were no microstructural changes, only the hole that was sealed with a plug and suffered a crevice corrosion mechanism.
145
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Corrosion
The macrography of a longitudinal section of the case shows one region where a through wall localized corrosion has occurred (in the left side of the image) and regions where the case was welded to a padeye, without any corrosion damage.
141
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Corrosion
The case where the electronic device was installed suffered a localized corrosion that allowed the seawater to wet the internal side, destroying it. The position where the leakage occurred originally presented a hole that was sealed with a plug and the corrosion occurred in a crevice condition.
166
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Aspect Before AnalysisDf - Localized Corrosion

+5 more from this case →

ML00086 — Intergranular Corrosion of Sensitized 304SSM - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
The low magnification image of the internal surface of the tube, in position 2, shows several points of localized corrosion, with intergranular morphology.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Surface Aspect by SEMDf - Intergranular Corrosion
Micrography of a longitudinal section of the tube in position 2, presenting thinning by intergranular corrosion at the internal surface.
193
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
Micrographic detail of the intergranular corrosion at the internal surface of the tube in position 2. Several grains were already removed by the corrosion.
171
VIEW
ML00086 / Nov.2017
Intergranular Corrosion of Sensitized 304SS
M - Austenitic Stainless SteelP - Seamless tubeAp - Heat ExchangerCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion
ML00050 — Fatigue Failure of a 316SS Pressure StabilizerM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Aspect of the equipment presenting a through wall cracking at the margin of the fillet weld.
143
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - Cracking
The macrography of a transverse section of the shell to flange weld (Lepto's etch) shows that the cracking occurred through the shell plate thickness, at the margin of the fillet weld.
93
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Transverse Section AspectDf - Cracking
Fracture surface after opening the shell cracking, presenting fatigue striation. The fracture presents also foreign particles.
132
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fatigue Striation