Intergranular Cracking

10 cases · 25 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Hydrogen Embrittlement clear all

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Micrography of a longitudinal section of the bolt, in a position close to the fracture (top) and bolt surface (left ), presenting several secondary intergranular cracks.
57
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Intergranular Cracking
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranuar, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
37
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
The fractography by SEM shows intergranular fracture close to the external surface of the pin.
93
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
Micrographic detail of an intergranular secondary crack (adjacent to the broken surface) propagating from the hard chromium layer.
75
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Fractographic analysis of the pin showing a region of predominantly intergranular fracture micromechanism.
46
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Surface Aspect by SEMDf - Intergranular Cracking
Micrographic detail of the longitudinal section of the link, presenting internal cracks of intergranular morphology, typical of a hydrogen assisted mechanism.
52
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks.
54
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Fractographic aspect of the broken fastener, at the surface, showing na intergranular morphology typical of a hydrogen assisted mechanism of a high strenght steel under cathodic protection.
224
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking

More from these cases

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the secondary intergranular cracks close to the surface of the bolt, where the fracture occurred.
56
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Intergranular Cracking
Micrographic detail of the intergranular cracks in the transition between the threaded body and the head of the non broken bolt, indicating that this bolt was also embrittled and could fail soon.
48
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the stud at the fracture (top of the figure) of a brittle intergranular aspect.
24
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
ML00009 — Hydrogen Cracking of a 5" Drill Pipe S135M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by SEM of the intergranular fracture close to the external surface of the pin.
83
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
Micrography of a longitudinal section of the pin, at the fracture position, showing the main fracture surface and secondary cracks associated to a segregation band, with an intergranular morphology.
49
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
ML00088 — Hydrogen Cracking of an API 5D S135 Drill PipeM - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of a secondary intergranular cracking at the pin longitudinal section (transverse to the fracture).
38
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
ML00079 — Hydrogen Cracking of a Maritime Chain LinkM - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Micrographic detail of the longitudinal section of the link, close to the fracture surface, presenting the intergranular morphology of the secondary cracks, parallel to the fracture.
29
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of the intergranular secondary cracks, parallel to the fracture, typical of a hydrogen assisted cracking.
29
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of the intergranular secondary cracks, parallel to the fracture, typical of a hydrogen assisted cracking. Close to the cracking it is possible to see an elongated inclusion, probably of a sulfide type.
26
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Micrography by SEMDf - Intergranular Cracking
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks. There is a large amount of delta phase precipitated intergranular and intragranluar.
49
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched MacroDf - Intergranular Cracking
ML00074 — Hydrogen Cracking of a 17-4 PH Subsea BoltM - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of intergranular cracks close to the fracture of the bolt, near the bolt surface where the macroscopi aspect was brittle.
82
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
The micrography, in the "as polished" condition, of the longitudinal section of the bolt showing that there are non-continuous longitudinal cracks, intergranular, associated to regions of impurities, probably segregation bands, as evidenced by the grey elongated sulfide inclusions.
76
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Intergranular Cracking
Micrographic detail of the longitudinal cracks in the middle of the bolt, that generaate the secondary cracks that appear at the fracture surface.
78
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking