Hydrogen

7 cases · 31 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Capture method: Optical Microscope Detail focus: Sampling and Analysis clear all

Hydrogen — sub-branches

Hydride Formation 3Hydrogen Embrittlement 14

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Low magnification micrography transverse to the fillet weld in the pipe. The pipe base metal is to the bottom of the figure and the weld metal is to the top. The heat affected zone in the middle, shows a coarse grain size structure.
59
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Welded Joint
Micrography of a longitudinal section, in the center, of the broken 5/8" bolt, presenting an aged martensitic structure. There are vertical "lines" that correspond to segregation bands due to the forming direction. These bands are evident only using low magnification microscopy.
168
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the pin, in the center. The low carbon content of the steel in the center of the pin makes the structure bainitic even though it was quenched and tempered after carburizing.
80
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, as polished, presenting brittle Intergranular and transgranular cracks, transverse to the bolt axis.
94
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Longitudinal Section
The longitudinal section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg). Previous austenite grains are elongated.
55
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the longitudinal section of the bolt, at the bottom of the thread fillet, showing that the fracture is intergranular in this position.
71
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section

More from these cases

ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Low magnification micrography showing the weld metal, full of pores, indicating that the field welding was not properly shileded.
50
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Coarse grains in the heat affected zone.
46
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone
Micrography of the weld metal at the fillet weld where the cracking started, showing several brittle microcracks that corresponds to the regions where the fractography showed secondary crackis.
35
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Micrographic detail of the weld metal brittle microcracks, in regions with hydrides formation.
32
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Brittle crack in the surface of the welded joint, at the heat affected zone close to the fusion line.
30
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone

+6 more from this case →

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the 5/8" bolt, at the bottom of the thread, presenting a refined structure compared to the center of the bolt and a mark at the thread flank that was probably created during tightening of the bolt.
95
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, close to the fracture surface (top of the figure), The fracture started at the surface (left side) in a position close to the bolt body to bolt head transition.
58
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Longitudinal Section
Micrography of a longitudinal section, in the center of a non-broken bolt that operated in the same assembling, presenting an aged martensitic structure, similar to the broken bolt.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the non-broken 5/8" bolt, at the transition between the threaded body and the head, showing a variation in the grain size (of the previous austenite) and evidences of a deformed structure at this transition.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Micrographic detail a longitudinal section of the pin, at the surface, showing the case hardened. The pin carburized, quenched and tempered structure presents a gradient of carbon content and consequently a gradient of martensitic structure and hardness. Close to the surface the hardness level is 742 HV1 .
87
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - At the Surface
ML00077 — Hydrogen Cracking of LAS Subsea BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the bolt, showing the (secondary) crack propagating, transverse to the bolt, from a thread fillet.
91
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the (secondary) crack propagating transverse to the bolt, from a thread fillet.
91
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the (secondary) crack propagating transverse to the bolt, from a thread fillet.
80
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the banded region, with microhardness identations indicating that the longitudinal bands are harder than the rest of the structure. The measurements in the band are 466, 447 and 460 HV50g; and out of the band are 358, 360 and 362 HV50g, from the top to the bottom.
86
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Microhardness Indentations
ML00076 — Hydrogen Cracking of a 17-7 PH Subsea SpringM - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the strain hardened aged martensitic structure. Small aligned delta ferrite islands can be seen.
51
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The transverse section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg).
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrographic detail of the strain hardened aged martensitic structure.
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrographic detail of the spring wire surface, far from the fracture, showing several small intergranular cracks.
40
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - At the Surface