Hydrogen

11 cases · 34 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Detail focus: Sampling and Analysis clear all

Hydrogen — sub-branches

Hydrogen Embrittlement 11

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Micrography of a longitudinal section, in the center, of the broken 5/8" bolt, presenting an aged martensitic structure. There are vertical "lines" that correspond to segregation bands due to the forming direction. These bands are evident only using low magnification microscopy.
168
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Aspect of the broken stud that was fastening a flanged line in a subsea body (tapped hole) using a nut. The fracture, transverse to the stud axis, occurred exactly at the body to flange interface. Adjacent to the fracture, all thread fillets (positioned inside the flange hole) presented cracks at the bottom of the thread. The stud was operating during seven years and was not corroded, indicating it was protected by the anodes. There are also deposits in the fillets suggesting the cathodic protection was effective even inside the flange hole.
799
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Aspect of the broken bolt, 5/8" Allen, socket head cap screw, originally 1 3/4" long, broken in subsea service under cathodic protection. The bolt presents a zinc coating.
116
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Aspect of the fracture that occurred in the connection between the pin of one DP and the box of other DP, in the pin side. The photo presents the pin still connected in the box. The flat fracture indicates a brittle behavior.
641
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Macrography of the longitudinal section of the tool joint, assembled. The pin is still attached to the box end of the other drill pipe in the column, showing that the pin fractured in the region of external diameter transition (right side of the figure), where the box was probably touching the pin shoulder. Interesting to note that the inner diameter still presents a sound coating.
73
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Longitudinal Section AspectDf - Longitudinal Section
Aspect of the broken bolt 1 1/2" nominal diameter, after a short time in service (non residente subsea equipment) under cathodic protection. The bolt broke at the thread fillet, close to the head.
800
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Brittle aspect of the failure of the conector in the male thread. Both sides of the fracture.
96
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
Aspect of the bolt fracture. The fracture appearance is irregular and there are several secondary cracks from thread fillets.
245
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View

More from these cases

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the 5/8" bolt, at the bottom of the thread, presenting a refined structure compared to the center of the bolt and a mark at the thread flank that was probably created during tightening of the bolt.
95
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, close to the fracture surface (top of the figure), The fracture started at the surface (left side) in a position close to the bolt body to bolt head transition.
58
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Longitudinal Section
Macrography of the longidutinal section of a non broken allen bolt, at the threaded body to bolt head transition. The granular structure is different through the bolt, with refined structure in the threaded body and coarse at the transition.
44
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched MacroDf - Longitudinal Section
Micrography of a longitudinal section, in the center of a non-broken bolt that operated in the same assembling, presenting an aged martensitic structure, similar to the broken bolt.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the non-broken 5/8" bolt, at the transition between the threaded body and the head, showing a variation in the grain size (of the previous austenite) and evidences of a deformed structure at this transition.
41
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Aspect of the fracture of a small Allen bolt, nominal diameter 5/8" 1 3/4" long, class 12.9, that was operating in subsea environment during 5 years. The fracture is rusted but the thread still presents the zinc coating.
81
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Aspect Before AnalysisDf - General View
ML00074 — Hydrogen Cracking of a 17-4 PH Subsea BoltM - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fracture view presenting two diferente aspects, brittle in the bottom of the figure and in the center (most part of the fracture) and ductile in the top of the figure. Nominal diameter of the bolt 1 1/2".
203
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fracture Surface AspectDf - General View
Macrography of a longitudinal section of the broken bolt, at the fracture position, showing that the fracture is partially flat (left side), where the macroscopically aspect is brittle, and a final ductile fracture (right side). Interesting to note that there is a large longitudinal crack, secondary (transverse to the fracture surface).
143
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched MacroDf - Longitudinal Section
Micrography of the longitudinal section of the bolt, at the bottom of the thread fillet, showing that the fracture is intergranular in this position.
71
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
ML00077 — Hydrogen Cracking of LAS Subsea BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
The longitudinal macrosection shows the fracture appearance, irregular, and a lot of secondary cracks transverse to the bolt axis, and longitudinal.
126
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Longitudinal Section AspectDf - Longitudinal Section
Several secondary cracks in the broken bolt, responsible for the irregular shape of the fracture, that presentes brittle cracks in the transverse and longitudinal directions.
109
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Longitudinal Section AspectDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, as polished, presenting brittle Intergranular and transgranular cracks, transverse to the bolt axis.
94
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Longitudinal Section
Micrography of a longitudinal section of the bolt, showing the (secondary) crack propagating, transverse to the bolt, from a thread fillet.
91
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the (secondary) crack propagating transverse to the bolt, from a thread fillet.
91
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Longitudinal Section

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