Scanning Electron Microscope

8 cases · 27 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Tempered Martensite Standard: UNS clear all

Scanning Electron Microscope — sub-branches

Fractography by SEM 11Kalling Etched Micrography by SEM 5Micrography by SEM 3Nital Etched Micrography by SEM 1Surface Aspect by SEM 7

Results

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Aspect by scanning electron microscopy of the brittle fracture surface. in a low magnification view. The fracture presents smashed regions (conditions imposed after the fracture was opened) in the region where the chevron marks indicate it is the failure starting point.
26
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Brittle Fracture
Fractographic aspect of the stud fracture surface, by scanning electron microscopy, close to the bottom of the thread fillet. In the center of the image it is possible to see secondary cracks with intergranular morphology.
59
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranular, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
517
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fracture
Aspect of the fracture surface of the bolt, after cleaning with a plastic brush. Although there is a layer of oxides it is possible to see the intergranular morphology of the fracture, typical of a hydrogen embrittlement mechanism.
1154
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic image by scanning electron microscope (SEM) of the ring surface that presented pites under fouling deposits.
522
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Micrographic detail of the intergranular secondary cracks, parallel to the fracture, typical of a hydrogen assisted cracking. Close to the cracking it is possible to see an elongated inclusion, probably of a sulfide type.
26
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Micrography by SEMDf - Intergranular Cracking
Fusion line micrographic detail. The weld metal is in the right and HAZ in the left.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Fusion Line
Tempered martensitic microstructure of the knife observed in a transverse section micrography. There are also secondary carbides (white globules) that increase the material wear resistance.
254
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite

More from these cases

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Observing in higher magnification it is possible to see that the fracture presents a mixture of ductile and brittle micromechanisms. The intergranular mechanism indicates that the material is embrittled and the dimples indicate localized overloading conditions.
32
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Fracture
Detail of the ductile dimples and the brittle intergranular micromechanisms. This evidence (a mixture of mechanisms) suggests that the embrittlement is localized in some regions of the material.
34
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Fracture
Scanning electron microscope fractographic detail of the brittle intergranular micromechanism.
40
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Intergranular Fracture
Scanning electron microscope fractographic detail of the ductile dimples.
26
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Fractography by SEMDf - Dimples
ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by scanning electron microscopy of the secondary cracks with intergranular morphology.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Secondary Cracks
Micrography of the bottom of the thread fillet, presenting secondary cracks of intergranular morphology, propagating transverse to the stud axis, but presenting longitudinal openings.
28
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by SEMDf - Cracks
ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranuar, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
37
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Detailed aspect of the fracture surface of the bolt, evidencing the intergranular morphology of the fracture (although with an oxide scale), typical of a hydrogen embrittlement mechanism.
114
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Microscopic details of the ring surface showing the fouling at the surface and localized corrosion under the deposits.
42
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Higher magnification of the localized corrosion, showing that there are cracks at the margin of the corroded region.
39
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
SEM image showing a branching surface crack extending from a region of granular corrosion deposits into the polished substrate.
32
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
Intergranular morphology inside the pitting and evidences of chemical attack (dissolution).
36
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Surface Aspect by SEMDf - Pitting
ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the base metal tempered martensite.
24
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Base Metal
Micrographic detail of the weld metal tempered martensitic microstructure.
25
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by SEMDf - Weld Metal
ML00054 — Cutlery CorrosionM - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Detail of the tempered martensitic microstructure with secondary carbides of the knife, observed in a transverse section micrography.
206
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite
Aspect of the rusted surface after cleaning, showing adhered products at the surface, in regions where the passive layer was destroyed and pitting corrosion occurred.
184
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Corrosion
Detail of the rusted surface. EDS analysis inside the pitting shows a high Cl peak (the bright aspect inside the pitting), indicating that the salt over the surface was responsible for destroying the passive layer and the localized corrosion occurred.
172
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Surface Aspect by SEMDf - Corrosion
Micrographic aspect of the pitting corrosion at the knife surface. It is possible to see the typical pitting aspect of a localized corrosion that appears as a small dot at the surface but it is a big crater under the surface.
185
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Micrography by SEMDf - Pitting
Detail of the micrographic aspect of the pitting corrosion at the knife surface.
168
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Micrography by SEMDf - Pitting