Scanning Electron Microscope

74 cases · 354 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage clear all

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 5Fractography by SEM 166Kalling Etched Micrography by SEM 2Micrography by SEM 50Nital Etched Micrography by SEM 39Surface Aspect by SEM 92

Results

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SEM fractograph at 1200x magnification showing an intergranular fracture surface with angular, faceted grains and fine feather-like markings.
86
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
The fracture surface is flat, shows the graphite nodules and cleavage of the ferritic microstructure, indicating that the material have exceeded the capacity to acomodate the stress.
944
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
External surface aspect of the flange showing preferential dissolution, responsible for nucleation of the through wall cracking.
245
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Surface Aspect by SEMDf - Preferential Dissolution
Regions of the pin thread presenting pitting corrosion.
635
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Localized Corrosion
The fracture surface of the main pipe is presented in low magnification (external pipe surface in the top) showing a flat propagation starting from the contour of the weld margin.
173
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Margin of the Weld Crack
Aspect of the internal surface of the pipe at the welded region, showing the interface of the thinning area in the weld and the pipe base metal.
128
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Surface Aspect by SEMDf - Localized Thinning
Casting defect identified in the micrographic section, as polished, of the sample removed from the blade. The total lenght of the defect detected by magnetic particle during inspection is 10 mm.
1041
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Micrography by SEMDf - Void
After opening the crack the fracture surface presented different aspects close to the internal surface and through the wall propagation. Intergranular at the surface, showing intergranular SCC mechanism, and transgranular with striation, showing the contribution of pulsing loads.
101
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Through Wall Cracking

More from these cases

ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Microscopic detail of the transgranular striation in the fracture surface.
78
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Fracture
ML00040 — Brittle Fracture of a Valve StemM - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Detail of the cleavage micromechanism.
195
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
ML00002 — Preferential Dissolution and Cracks in SDSSM - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Detail of the region at the flange external surface where the material is suffering the preferential corrosion.
177
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Surface Aspect by SEMDf - Preferential Dissolution
Micrographic detail of the through wall cracking in the middle of the thickness, showing that the cracking is associated to ferrite network in the (super)duplex microstructure.
128
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Micrography by SEMDf - Crack
Micrographic detail of the cracking, associated to the ferrite network, that presents both corrosion (preferential dissolution) and fracture (clevage) aspects.
128
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Electrolytic Etch Micrography by SEMDf - Crack
The fracture surface, although presenting a large amount of corrosion products, shows also evidences of a brittle behavior with regions of cleavage micromechanism.
116
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Fractography by SEMDf - Cleavage Facets
Micrographic detail of the ferrite network with evidences of precipitation/formation of detrimental phases. NaOH solution was adopted for the electrolytic etching.
86
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Electrolytic Etch Micrography by SEMDf - Delta ferrite

+2 more from this case →

ML00016 — SCC in Free Cutting 303SSM - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Regions of the localized corrosion spots associated to non metallic inclusions.
123
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Non Metallic Inclusions
Detail of the pin surface showing that the material easily cracks because it presents regions of localized corrosion.
45
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Fracture
ML00006 — Vibration Induced Fatigue in 304SSM - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Fracture surface micromechanism by striation, evidence of FATIGUE.
158
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
Fracture surface micromechanism by striation, evidence of FATIGUE.
147
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
ML00005 — Environmental Hydrogen Damage in Ti PipeM - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Region of the localized thinning at the weld metal, in a metallographic section, as polished. In the base metal the hydride layer is continuous and no thinning is evident (left side of the figure) and in the weld metal it is detached and cracked (right side of the figure).
107
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Localized Thinning
Hydride layer at the internal surface of the pipe base metal, after Kroll etch.
71
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Hydride Formation
Detail of the hydride layer at the internal surface of the pipe base metal, after Kroll etch.
62
VIEW
ML00005 / Apr.2017
Environmental Hydrogen Damage in Ti Pipe
M - Unalloyed TitaniumP - Longitudinal Seam Welded PipeAp - PipingCd - Hydride Formation
Cm - Micrography by SEMDf - Hydride Formation
ML00017 — Casting Defect in CA6NMM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Region of a casting void in the blade. As polished.
33
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Micrography by SEMDf - Void
ML00011 — Intergranular SCC of Pure NickelM - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
After opening the crack the fracture surface presented different aspects close to the surface, initiation mechanism, and through the wall propagation. Detail of the intergranular cracking mechanism close to the internal surface.
98
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Intergranular Cracking
After opening the crack the fracture surface presented different aspects close to the internal surface, in the initiation, and through the wall propagation. Detail of the transgranular striation, showing the contribution of pulsing loads.
98
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Fatigue Striation
After opening the crack the fracture surface presented different aspects close to the internal surface, in the initiation, and through the wall propagation. Detail of the transgranular striation, showing the contribution of pulsing loads.
82
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Fractography by SEMDf - Fatigue Striation