Scanning Electron Microscope

8 cases · 17 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Standard: UNS Detail focus: Microstructure clear all

Scanning Electron Microscope — sub-branches

Electrolytic Etch Micrography by SEM 4Kalling Etched Micrography by SEM 2Micrography by SEM 8Nital Etched Micrography by SEM 2Surface Aspect by SEM 1

Results

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Micrographic detail of the martensitic structure, clearly obtained from a refined previous austenitic structure .
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
Micrography, by scanning electron microscopy. The alloy is a precipitation hardened material, and the stains at the surface are associated to differential etching in second phases and inclusions.
35
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Micrography by SEMDf - Granular structure
Micrographic detail by scanning electron microscopy of the interface between the two thermal spray layers, the first one in stainless steel (bottom of the figure) and the second one, at the surface,in tungsten carbide (top of the figure). The composition of the first layer is similar to the base metal (lean duplex) and the composition of the second layer is WC in a Co matrix.
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Thermal Spray Layer
Micrography of the plate in a section, showing the alpha grains plus beta phase microstructure in the middle of the thickness. The sample was mechanically-electrolitically polished and etched with HF+HNO3+H2O solution.
27
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by SEMDf - Alpha and Beta
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
92
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Tempered martensitic microstructure of the knife observed in a transverse section micrography. There are also secondary carbides (white globules) that increase the material wear resistance.
254
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite
Regions of the localized corrosion spots associated to non metallic inclusions.
123
VIEW
ML00016 / Apr.2017
SCC in Free Cutting 303SS
M - Austenitic Stainless SteelP - Machined PartAp - OffshoreCd - Stress Corrosion
Cm - Surface Aspect by SEMDf - Non Metallic Inclusions
Micrographic detail of the ferrite network with evidences of precipitation/formation of detrimental phases. NaOH solution was adopted for the electrolytic etching.
86
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - Electrolytic Etch Micrography by SEMDf - Delta ferrite

More from these cases

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the martensitic structure.
19
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by SEMDf - Martensite
ML00145 — Impact of a .380 Winchester on 6061 T6 PlateM - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Micrographic detail, by scanning electron microscopy, of the precipitation hardened granular structure. The stains are preferential etch of second particles.
32
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Micrography by SEMDf - Aligned particles
ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrographic detail of the first thermal spray layer, in stainless steel with the same composition of the base metal (lean duplex).
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Thermal Spray Layer
Micrographic detail, by scanning electron microscopy, of the duplex, austenitic and ferritic, structure with sigma phase.
16
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - Electrolytic Etch Micrography by SEMDf - Sigma
ML00144 — Impact of a .380 Winchester on Ti64 PlateM - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Micrographic detail by SEM, showing the beta phase EDS analysis was conducted in this microstructure and the results indicated 90.8%Ti + 6.8%Al + 2.4%V for the alpha phase (the dark grains as a matrix); and 84.7%Ti + 5.2%Al + 8.8%V + 1.2%Fe for the beta phase (light with aicular morphology inside the phase).
25
VIEW
ML00144 / Aug.2018
Impact of a .380 Winchester on Ti64 Plate
M - Ti6Al4VP - Rolled PlateAp - StructureCd - Non-Pierced
Cm - Micrography by SEMDf - Alpha and Beta
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
85
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
High magnification details by scaning electron microscopy. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
81
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
Higher magnification detail of the sigma phase by scaning electron microscopy.
76
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - Micrography by SEMDf - Sigma
ML00054 — Cutlery CorrosionM - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Detail of the tempered martensitic microstructure with secondary carbides of the knife, observed in a transverse section micrography.
206
VIEW
ML00054 / Dec.2018
Cutlery Corrosion
M - Martensitic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Pitting Corrosion
Cm - Kalling Etched Micrography by SEMDf - Martensite