Fractography by SEM

31 cases · 107 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranular, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
517
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Fracture
Aspect of the fracture surface of the bolt, after cleaning with a plastic brush. Although there is a layer of oxides it is possible to see the intergranular morphology of the fracture, typical of a hydrogen embrittlement mechanism.
1154
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
The hose connector fracture surface presented different fracture micromechanisms associated to the microstructure: inclusion decohesion, small regions of intergranular fractures (probably due to cementite at grain boundaries), and cleavage of the ferritic structure. All these mechanisms are brittle.
560
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Brittle Fracture
The fractographic analysis of the pin showed fatigue striation at the subcritical propagation region.
75
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Fractography by SEMDf - Fatigue Striation
The through wall cracking was opened by citting the two sides and the aspect was characterized by SEM. Although there was a film at the fracture surface, probably because the fitting was removed from service some time after it was leaking, the fracture micromechanism is by quasecleavage, typical of a stress corrosion cracking.
56
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material.
31
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
The fractography by SEM shows intergranular fracture close to the external surface of the pin.
93
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
Fractographic analysis of the pin fracture surface showing inter and transgranular morphologies of fracture micromechanisms.
53
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Brittle Fracture

More from these cases

ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Fractographic analysis by scanning electron microscopy of the stud fracture surface after opening the cracks. Brittle intergranular morphology with dimples and quasecleavage micromechanisms indicate that the internal cracks, intergranuar, occurred by a hydrogen embrittlement effect during electroplating, and the ductile aspects are probably associated to overloading during torque.
37
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Detailed aspect of the fracture surface of the bolt, evidencing the intergranular morphology of the fracture (although with an oxide scale), typical of a hydrogen embrittlement mechanism.
114
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Fracture
ML00103 — Brittle Fracture of a Free-Cutting ConnectorM - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Details of the inclusion decohesion and cleavage.
89
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Cleavage Facets
Details of the cleavage fracture in the ferritic structure.
86
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Brittle Fracture
Details of the intergranular fracture, probably associated to cementite at grain boundaries.
68
VIEW
ML00103 / Nov.2017
Brittle Fracture of a Free-Cutting Connector
M - Low Carbon SteelP - Machined PartAp - ShipCd - Brittle Fracture
Cm - Fractography by SEMDf - Intergranular Fracture
ML00085 — Corrosion Fatigue of a Martensitic SS PinM - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
The fractographic analysis of the pin showed ductile final fracture, by dimples.
76
VIEW
ML00085 / Nov.2017
Corrosion Fatigue of a Martensitic SS Pin
M - Martensitic Stainless SteelP - Forged PinAp - O&G Well DrillingCd - Corrosion Fatigue
Cm - Fractography by SEMDf - Dimples
ML00080 — MIC of Stacking Disc SpringsM - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Microscopic detail of the fracture surface in the position where the fracture is intergranular, probably due to the MIC attack creating an embrittled condition of the material. A surface film is evident in this position suggesting that the fracture remained open and exposed to the environment during a certain time before the failure was detected.
29
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Fracture micromechanisms. Intergranular fracture in the top of the figure (close to the groove) and transgranular fracture in the bottom of the figure, where the mechanism changed to transgranular by quasecleavage.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Intergranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
27
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
Microscopic detail of the fracture surface where it is transgranular, by quasecleavage. This aspect is similar to the one expected for this high strenght material without any embrittlement.
26
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Fractography by SEMDf - Transgranular Fracture
ML00009 — Hydrogen Cracking of a 5" Drill Pipe S135M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Fractographic detail by SEM of the intergranular fracture close to the external surface of the pin.
83
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Intergranular Cracking
The fractography by SEM shows quasecleavage mechanism in the middle of the wall thickness of the pin.
81
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Cracking
Fractographic detail by SEM of the quasecleavage mechanism in the middle of the wall thickness of the pin.
74
VIEW
ML00009 / Sep.2017
Hydrogen Cracking of a 5" Drill Pipe S135
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Fractography by SEMDf - Transgranular Crack