Optical Microscope

109 cases · 908 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Optical Microscope — sub-branches

As polished micrography 64Chromic Acid Electrolytic Etched 6Eletrolytically Etched Micrography by OM 6FeCl3+HCl+Ethanol Etched Micro 14FeCl3+HCl+H2O Etched Micro 12Glyceregia Etched Micrography by OM 6H2SO4+HNO3+H3PO4 Etched Micro 3Kalling Etched Micrography by OM 108Keller Etched Micrography by OM 46Kroll Etched Micrography by OM 5Micro by OM, picric acid+FeCl3+H2O etch 1Micrography by OM 53Micrography by OM using A262 Method A 44Micrography by OM, HF + HNO3 + H2O etch 6NaOH Electrolytic Etched Micro 47Nital Etched Micrography by OM 460Oxalic Acid Electrolytic Etch 27

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The micrography of the pipe in the longitudinal section shows an aligned structure.
60
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of the shell plate in the longitudinal section. Ferritic-perlitic microstructure.
96
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Typical branched stress corrosion cracks in a low carbon steel, ferritic-pertlitic structure. The cracks are filled with corrosion products.
771
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Tempered martensitic structure of the plate base metal.
93
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
The micrography of the tube shows a granular structure and light deformation lines. No evidences of corrosion from the external surface (upper side of the figure) or internal surface (lower side of the figure).
440
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Longitudinal Section
Transverse section of the blade showing large grains of this poliycristaline cast material.
421
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Coarse Structure
The micrography of a transverse section of the shaft shows the granular austenitic structure close to the surface of the shaft.
67
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
The cast iron microstructure is predominatly ferritic with graphite nodules.
169
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Graphite in Nodules

More from these cases

ML00053 — SAW Longitudinal Seam of X70 PipeM - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Detail of the microstructure in the center of the plate, in the longitudinal section. The structure is refined and presents different ferritic grain sizes.
49
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Detail of the microstructure in the center of the plate, in the longitudinal section. The ferritic structure is refined and presents different grain sizes. Carbides are presented in different morphologies (perlite, precipitated) and there are probably microphases (aligned in a central segregation line).
55
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrographic detail of the fusion line of the second pass (not reheated). The HAZ is bainitic and the weld metal microstructure is predominantly formed by acicular ferrite.
51
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line
Center of the weld in the second pass. Columnar grains of the previous austenite.
45
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Weld Metal
Fusion line of the first pass (reheated in high temperature). The HAZ is bainitic and the weld metal microstructure is predominantly formed by acicular ferrite.
43
VIEW
ML00053 / Mar.2017
SAW Longitudinal Seam of X70 Pipe
M - Microalloyed SteelP - Longitudinal Seam Welded PipeAp - SubseaCd - Welding
Cm - Nital Etched Micrography by OMDf - Fusion Line

+6 more from this case →

ML00019 — Transgranular SCC in Boiler Steam DrumM - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Micrographic detail of the shell plate in the longitudinal section. Ferritic-perlitic microstructure.
89
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the cracking showing the branched nature, typical of a stress corrosion cracking. The cracks started from the internal surface of the steam drum.
94
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrographic detail of the cracking showing the branched nature, typical of a stress corrosion cracking. The cracks presented a transgranular morphology
86
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
Micrographic detail of the transgranular stress corrosion cracking.
80
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
Micrographic detail of the transgranular stress corrosion cracking.
157
VIEW
ML00019 / Apr.2017
Transgranular SCC in Boiler Steam Drum
M - CMn SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Transgranular Crack
ML00018 — SCC in Boiler Steam DrumM - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Ferritic perlitic structure of the shell plate.
207
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the crack at the internal surface of the steam drum. The shell plate presents a ferritic perlitic structure.
162
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrography of a crack, in a sample as polished, presenting the opened crack.
144
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Micrography by OMDf - Branched Cracks
Stress corrosion cracks propagating in the ferritic-perlitic structure.
120
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Branched Cracks
Micrography of a crack, as polished, presenting the cracks filled with corrosion products.
100
VIEW
ML00018 / Apr.2017
SCC in Boiler Steam Drum
M - Low Carbon SteelP - Rolled PlateAp - BoilerCd - Stress Corrosion
Cm - Micrography by OMDf - Branched Cracks

+2 more from this case →

ML00010 — Cold Cracks in a Gouged Weld MetalM - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Detail of the tempered martensitic structure of the plate base metal. Hardness level of 27 HRc.
92
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Base Metal
Low magnification micrography of a transverse section of the weld at the heat affected zone region. The macrosection was hardness tested and the base metal hardness is 27HRc, the HAZ is 32HRc and the weld metal is 45HRc, revealing something wrong in the weld metal at the position close to the cracked area.
79
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Transverse Section
High temperature heat affected zone of the plate, welded in repair. The micrography was taken from a sample collected close to the cracked region, but not containing any macroscopic cracking.
76
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
Detail of the high temperature heat affected zone of the plate, welded in repair.
69
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Heat Affected Zone
The weld metal, hard, presented a martensitic structure, probably due to the localized increase in carbon content, from the unsuitable carbon arc gouging procedure.
63
VIEW
ML00010 / Oct.2017
Cold Cracks in a Gouged Weld Metal
M - Low Alloy Low Carbon QTP - Rolled PlateAp - OffshoreCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Weld Metal

+5 more from this case →

ML00043 — CuNi Condenser TubeM - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
The material structure is monophasic.
110
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Single phase
Detail of the structure at the surface.
79
VIEW
ML00043 / Apr.2017
CuNi Condenser Tube
M - CupronickelP - Seamless tubeAp - Heat ExchangerCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - At the Surface
ML00042 — Gas Turbine Blade IN 939, CoatedM - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Micrography close to the surface of the blade, showing the diffusion coating (aluminum base alloy) that is still sound. No strong oxidation or erosion was detected.
53
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Coating
Micrography as polished of the region where there was a refrigeration hole, presenting a cracking.
35
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - Micrography by OMDf - Cracking
The cracking from the refrigeration hole presents an intergranular morphology, as shown in the micrography of a transverse section of the blade.
35
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Intergranular Cracking
ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Micrographic detail of the granular austenitic structure close to the surface of the shaft.
64
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - At the Surface
Granular austenitic structure close to the surface of the shaft.
61
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Austenite
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft.
49
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
The micrography of a transverse section of the shaft shows a duplex grain size structure in the center of the shaft. This conditions was probably generated due to the delta phase presented in segregated bands in the center of the original bar.
56
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
Duplex grain size structure, austenitic. The small grains are probably due to the arresting effect of the delta phase during fabrication in high temperature.
47
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Duplex structure

+2 more from this case →

ML00040 — Brittle Fracture of a Valve StemM - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
The micrography of the stem at the fracture region shows a flat fracture with transgranular clevage at the ferritic structure.
137
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Fracture
Micrography presenting a detail of the fracture surface opening to the graphite nodules.
139
VIEW
ML00040 / Apr.2017
Brittle Fracture of a Valve Stem
M - Nodular Cast IronP - Valve StemAp - ShipCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Fracture