Optical Microscope

15 cases · 113 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Austenite Standard: A clear all

Optical Microscope — sub-branches

As polished micrography 4Eletrolytically Etched Micrography by OM 6Glyceregia Etched Micrography by OM 6Kalling Etched Micrography by OM 4Micrography by OM 8Micrography by OM using A262 Method A 58Nital Etched Micrography by OM 14Oxalic Acid Electrolytic Etch 13

Results

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Through wall cracking in the longitudinal seam weld of the fitting. Several cracks, longitudinal to the weld, were created by the connection of voids in the weld metal, associated to a strong microstructural evolution.
191
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Cracks
Micrography of a longitudinal section of the pipe showing that the carbon steel pipe is slightly banded and there is a decarburized layer at the solid solution welded interface. The stainless steel structure (in the right side of the figure) is not revealed using the Nital etch.
125
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the fatigue cracking at the margin of the flange to shell fillet weld.
484
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack
The micrography of the transverse section of the plate, as polished, close to the surface. The material presents intergranular corrosion and some grains were lost.
1184
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrography of the transverse section of the NEW TUBE, in the center of the thickness, showing the austenitic structure with primary carbides network.
410
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Austenitic with Primary Carbides
Longitudinal section of the main pipe showing as austenitic structure with small amount of delta ferrite, aligned. The white band in the center of the figure is a segregation band that was not fully etched.
133
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography of a transverse section of the pipe, presenting the pitting corrosion. As polished.
310
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OMDf - Pitting

More from these cases

ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrography of a transverse section of the seam weld, close to the internal surface, presenting several cracks perpendicular to the thickness.
37
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Close to the Internal Surface
Micrographic detail of the seam weld close to the internal surface, presenting the needles that are the result of microsctructural evolution and cracks filled with oxides.
36
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Close to the Internal Surface
Micrography of a transverse section of the seam weld, in the middle of the thickness, presenting several parallel cracks.
27
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - In the Center of the Thickness

+7 more from this case →

ML00056 — Seamless Tube Externally Cladded with SSM - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Micrography of a longitudinal section of the pipe showing the carbon steel pipe , internal.
122
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a longitudinal section of the pipe showing the stainless steel pipe , external.
99
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrographic detail of the interface in the longitudinal section of the pipe showing the Vickers (300g) microhardness values, close to the interface in the carbon steel side and in the stainless steel side. Although the Nital etch does not allow to reveal the structure in the stainless steel side, the high hardness values show that the structure is different.
113
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of the interface in the longitudinal section of the pipe showing the decarburized layer at the solid solution welded interface. The stainless steel structure (in the right side of the figure) is not revealed using the Nital etch.
80
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Clad Interface
Micrography of the interface between the carbon steel that is strongly etched by the electrolytic oxalic acid (in the left side of the figure) and the stainless steel, in the longitudinal section of the pipe. There is a strain hardened layer very close to the interface, at the stainless steel side.
79
VIEW
ML00056 / May.2018
Seamless Tube Externally Cladded with SS
M - Carbon Steel / Stainless SteelP - CladdingAp - Pulp and PaperCd - Removed From Service
Cm - Micrography by OM using A262 Method ADf - Longitudinal Section

+2 more from this case →

ML00050 — Fatigue Failure of a 316SS Pressure StabilizerM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
The shell plate micrography showed an austenitic structure.
101
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
The micrography of the welded joint between the flange and the shell, in a region that was through wall cracked, the fracture propagating in the shell plate base metal.
74
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Welded Joint
The micrography of the welded joint between the flange and the shell, in a region that was not yet macroscopically cracked, presented a fatigue crack from the margin of the fillet weld.
71
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Welded Joint
ML00015 — Intergranular Corrosion of 304SS PlateM - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
303
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Microstructure of the plate in the center of the ¼” thickness. Equiaxed austenitic grains with delta ferrite stringers and grain boundary carbide precipitation (sensitization).
201
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Precipitation
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region where it was detected intergranular corrosion up to 0,5 mm depth. As polished.
188
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic detail of intergranular corrosion, up to 0,5 mm depth. As polished.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OMDf - Intergranular Corrosion
Micrographic aspect of a longitudinal section of the plate, close to the surface, in a region with intergranular corrosion. Several loose grains were removed, indicating that the structure was embrittled by the intergranular corrosion.
171
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Corrosion

+4 more from this case →

ML00038 — Cast SS Tube for High Temperature ServiceM - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Micrography of the transverse section of the NEW TUBE, close to the external surface, showing the austenitic structure with primary carbides network.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects close to the external surface.
49
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Close to the External Surface
The micrography in the as polished condition of the NEW TUBE shows that there are no casting defects in the center of the thickness.
47
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Micrography by OMDf - Transverse Section
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE, in the center of the thickness, showing the austenitic structure with primary carbides network and secondary precipitation.
59
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Intragranular Secondary Precipitation
Micrography of the transverse section of the TUBE REMOVED FROM SERVICE,close to the external surface, showing the austenitic structure with coalesced carbides and secondary precipitation.
40
VIEW
ML00038 / Apr.2017
Cast SS Tube for High Temperature Service
M - Heat Resistant SteelP - Centrifugally Cast PipeAp - SiderurgyCd - Creep
Cm - Glyceregia Etched Micrography by OMDf - Close to the External Surface

+2 more from this case →

ML00006 — Vibration Induced Fatigue in 304SSM - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Longitudinal section of the main pipe showing as austenitic structure with small amount of delta ferrite, aligned (black dots).
117
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Austenite
Micrography transverse to the weld and to the fracture surface (right side of the figure).
116
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Fracture
Micrography of the section transverse to the weld and in a region close to the fracture surface (to the right side of the figure). The secondary fatigue microcracks are associated to the stress concentration raisers of the margin of the weld, irregular.
110
VIEW
ML00006 / Apr.2017
Vibration Induced Fatigue in 304SS
M - Austenitic Stainless SteelP - Longitudinal Seam Welded PipeAp - PipingCd - Vibration Induced Fatigue
Cm - Micrography by OM using A262 Method ADf - Fatigue Crack
ML00014 — Pitting Corrosion in 316SS PipeM - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Austenitic structure at the transverse section of the pipe, free from carbides.
277
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite
Austenitic structure, free from carbides, exactly in the region of the pitting, indicating that the corrosion is not associated to the material microstructure.
261
VIEW
ML00014 / Apr.2017
Pitting Corrosion in 316SS Pipe
M - Austenitic Stainless SteelP - Seamless PipeAp - FPSOCd - Pitting Corrosion
Cm - Micrography by OM using A262 Method ADf - Austenite