Optical Microscope

35 cases · 135 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Standard: AISI Detail focus: Microstructure clear all

Optical Microscope — sub-branches

As polished micrography 6Eletrolytically Etched Micrography by OM 2Kalling Etched Micrography by OM 5Micro by OM, HCl + Ethanol + Picric Acid 6Micrography by OM 2Micrography by OM using A262 Method A 15NaOH Electrolytic Etched Micro 3Nital Etched Micrography by OM 80Oxalic Acid Electrolytic Etch 16

Results

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Micrography presenting a tempered martensitic microstructure, with light etch in segregated bands.
74
VIEW
ML00182 / Jul.2022
Brittle Fracture of a LAS Fixing Rod
M - Low Alloy Medium Carbon QTP - StemAp - Mechanical IndustryCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Tempered Martensite
Detailed microstructure of the plate base metal, exposed to high temperature exhausting gases. Refined austenite, precipitation of carbides in the grain boumdaries and some cracks.
23
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of spring surface, showing the pits full of corrosion deposits and a small decarburized layer (probably from the manufacturing processes).
30
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Decarburized Surface
Metallographic detail of the longitudinal section of the clamp with a ferritic pearlitic structure.
32
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section of the tubing, showing the austenitic structure free from strain hardening and free from grain boundary carbides.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
Low magnification micrography of a longitudinal section of the valve body, in the center of the thickness. As expected for this high strength steel, the microstructure is martensitic, but with segregation bands.
48
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Banded Structure

More from these cases

ML00174 — Carburization of a 347 SS Welded JointM - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Detailed microstructure of the weld metal, exposed to high temperature exhausting gases. Austeno-ferritic structure and some cracks.
21
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Ferrite and Austenite
Microstructure of the heat affected zone (weld metal to the left side), exposed to high temperature exhausting gases. Large austenitic grain size and intergranular cracks fully opened and filled with oxides.
21
VIEW
ML00174 / Jul.2021
Carburization of a 347 SS Welded Joint
M - Austenitic Stainless SteelP - Fabrication WeldAp - EnergyCd - Carburization
Cm - Oxalic Acid Electrolytic EtchDf - Coarse Structure
ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the transverse section of the spring wire, martensitic.
24
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic structure, uniform through thickness.
17
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Metallographic detail of the ferritic perlitic structure.
31
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
53
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Micrographic detail of the austenitic structure, free from strain hardening and free from grain boundary carbides.
54
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
SAMPLE 1 AT 1 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular.
76
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 1 AT 1 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides.
72
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular. There are no variations in the microstructure comparing to sample 1.
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides. There are no variations in the microstructure comparing to sample 1.
43
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Precipitation
SAMPLE 3 AT 4 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation, but this micrography was obtained in the longitudinal section, presenting the plate alignment and was etched with NaOH, adopted to colour the sigma phase.
45
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - NaOH Electrolytic Etched MicroDf - Austenitic with Secondary Precipitation

+4 more from this case →

ML00162 — Valve Body Crack Growth from Weld DefectsM - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Micrography of a longitudinal section of the valve body presenting a martensitic microstructure. The structure is banded and the darker regions show inclusions (grey sulfides).
50
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic microstructure, in the longitudinal section. The hardness of the valve body is 34 HRc (Rockwell C) all through the thickness.
47
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the weld repair at the fusion line. Weld metal to the right and heat affected zone to the left.
37
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
Micrographic detail of the fusion line.
33
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line