Optical Microscope

162 cases · 600 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Detail focus: Microstructure clear all

Optical Microscope — sub-branches

As polished micrography 13Chromic Acid Electrolytic Etched 4Eletrolytically Etched Micrography by OM 4FeCl3+HCl+Ethanol Etched Micro 6FeCl3+HCl+H2O Etched Micro 17Glyceregia Etched Micrography by OM 5H2SO4+HNO3+H3PO4 Etched Micro 2Kalling Etched Micrography by OM 62Keller Etched Micrography by OM 7Kroll Etched Micrography by OM 3Micro by OM, HCl + Ethanol + Picric Acid 6Micrography by OM 17Micrography by OM using A262 Method A 39Micrography by OM, HF + HNO3 + H2O etch 6NH4OH+H2O+H2O2 Etched Micro 3NaOH Electrolytic Etched Micro 44Nital Etched Micrography by OM 329Oxalic Acid Electrolytic Etch 33

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Micrography of a longitudinal section of the tubing, showing the austenitic structure free from strain hardening and free from grain boundary carbides.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Low magnification micrography of a transverse section of the ring showing a dendritic structure.
64
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of the tranverse section of the tube, in the center of the thickness. There are small grains and large grains, characterizing a dual grain size. The large grains size is about 100 microns, more than 10 times larger than the average size of the smaller grains size.
101
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Dual grain sizes
The tube microstructure is ferritic-pearlitic, typical of this kind of material. No evidences of microstrutural changes were detected (no overheating, no decarburization).
177
VIEW
ML00163 / Jun.2020
Corrosion Fatigue of a Boiler Waterwall Tube
M - Low Carbon SteelP - Seamless tubeAp - BoilerCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
SAMPLE 1 AT THE FRACTURE - Micrography at the position where the thickness is reduced to zero. Side A to the bottom. The microstructure is austenite with intergranular and transgranular precipitation. The position of the zero thickness presents aspect of an intergranular fracture, and in side A there are several intergranular cracks from the surface.
83
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
Low magnification micrography of a longitudinal section of the valve body, in the center of the thickness. As expected for this high strength steel, the microstructure is martensitic, but with segregation bands.
48
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of a longitudinal section of the socket at the position where the fracture occurred. Uniform tempered martensitic structure. The hardness of this microstructure is 639 HV1Kg.
74
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite

More from these cases

ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Micrographic detail of the austenitic structure, free from strain hardening and free from grain boundary carbides.
54
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Micrography of a transverse section of the ring showing a cored alpha structure with segregation at interdendritic regions. This structure is in a region close to the ring surface.
52
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with strong segregation at interdendritic regions, and regions of a white structure at grain boundaries. This structure is in a region close to the center of the ring.
51
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrographic detail of the cored alpha structure with light segregation at intergranular regions (light layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the ring surface, where the solidification was quicker.
49
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
Micrographic detail of the cored alpha structure with strong segregation at intergranular regions (dark layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the center of the ring, where the solidification was slower.
47
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Micrographic detail of the alpha microstructure presenting dual grain sizes. Two different types of twins are presented in the structure: annealing twins and deformation twins, suggesting that the material was probably partially recristalized after cold deformation and stress relief treatment.
87
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Alpha
ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the valve wall 1" thick. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite is clean indicating that the homogeneization of a smaller thickness in the heat treatment is considered effective.
40
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the clean austenitic matrix, with delta ferrite in interdendritic spaces.
35
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
SAMPLE 1 AT 1 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular.
76
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 1 AT 1 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides.
72
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Austenitic with Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary precipitation, intergranular and intragranular. There are no variations in the microstructure comparing to sample 1.
48
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Secondary Precipitation
SAMPLE 2 AT 2 mm THICKNESS - Micrographic detail of the austenite with secondary precipitation. This oxalic acid electrolytic etch is revealing the integranular and transgranular (or intragranular) precipitation. In the grain boundaries it is possible to see: 1) a continuous network of carbide precipitation and 2) isolated islands of sigma phase. In the middle of the grains there are rounded and neddles like carbides. There are no variations in the microstructure comparing to sample 1.
43
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Intergranular Precipitation
SAMPLE 3 AT 4 mm THICKNESS - Micrography in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation, but this micrography was obtained in the longitudinal section, presenting the plate alignment and was etched with NaOH, adopted to colour the sigma phase.
45
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - NaOH Electrolytic Etched MicroDf - Austenitic with Secondary Precipitation

+4 more from this case →

ML00162 — Valve Body Crack Growth from Weld DefectsM - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Micrography of a longitudinal section of the valve body presenting a martensitic microstructure. The structure is banded and the darker regions show inclusions (grey sulfides).
50
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic microstructure, in the longitudinal section. The hardness of the valve body is 34 HRc (Rockwell C) all through the thickness.
47
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the weld repair at the fusion line. Weld metal to the right and heat affected zone to the left.
37
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
Micrographic detail of the fusion line.
33
VIEW
ML00162 / Apr.2020
Valve Body Crack Growth from Weld Defects
M - Low Alloy Medium Carbon QTP - Valve BodyAp - O&G Well DrillingCd - Fatigue Induced by a Defect
Cm - Nital Etched Micrography by OMDf - Fusion Line
ML00161 — Brittle Fracture of a High Strength SocketM - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Micrography of a longitudinal section presenting an uniform tempered martensitic structure.
81
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensitic structure.
80
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite
Brittle Fracture of a High Strength Socket
4
VIEW
ML00161 / Mar.2020
Brittle Fracture of a High Strength Socket
M - Medium Carbon Tool SteelP - ToolAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Martensite