Oxalic Acid Electrolytic Etch

2 cases · 9 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Welding clear all

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Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
904
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Low magnification micrography of a longitudinal section of the pipe at the interface,with oxalic acid electrolytic method that overetchs the low alloy steel structure (to the left side of the image), and reveals the structure of the clad interface.
49
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface

More from these cases

ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Micrography of a longitudinal section of the pipe at the interface,with oxalic acid electrolytic method that overetchs the low alloy steel structure (to the left side of the image), and reveals the structure of the clad plate interface, different at the position where it was metallurgically bonded to the the pipe (when it was still a low alloy plate - X65).
36
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Micrography of the metallurgically bonded interface of the internally cladded pipe. The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment.
35
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Micrographic detail of the metallurgically bonded interface of the internally cladded pipe. The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness very close to the interface (429 HV100g) is higher than the value of 358HV 100g ,obtained 0.2mm far from this region in the clad plate .
37
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
28
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
26
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Grain refined structure
ML00132 — Seamless Pipe Overlaid with Alloy 625M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Micrography of a longitudinal section of the pipe at the interface,with oxalic acid electrolytic method that reveals the structure of the clad interface. Celular structure and transgranular precipitation.
48
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Micrographic detail of a longitudinal section of the pipe at the interface,with oxalic acid electrolytic revealing the structure of the clad interface. Celular structure and transgranular precipitation.
44
VIEW
ML00132 / May.2018
Seamless Pipe Overlaid with Alloy 625
M - LAS / Ni AlloyP - Seamless PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface