Nital Etched Micrography by OM

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrography of a transverse section of the seamless pipe, presenting a ferritic-pearlitic structure.
84
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
109
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Longitudinal section micrography in a position of the thread, far from the failure. The stud presented a quenching and tempering structure and the thread was machined.
84
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrography of an axial section of the roller bearing, at the external surface, where the hardness level was about 64 HRc (higher than the limit of 58HRc to 62 HRc).
86
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Close to the External Surface
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
134
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrographic aspect, after Nital etching, of the longitudinal section of the cylinder, at the surface, in a region where the damage is in the begining. There are two layers at the surface. A first Ni layer, 160 microns thick and 300HV average hardness, over the low carbon steel substrate, 200HV average hardness, and a chromium plated layer, 250 microns thick and 1100HV average hardness.
59
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corrosion
Micrography of the longitudinal section of the stud presenting a tempered martensite structure, slightly banded. Hardness 45 HRc.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the longitudinal section of the bolt showing a martensitic structure, with segregation bands evidenced by the chemical etch.
99
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure

More from these cases

ML00149 — Vibration Induced Fatigue in a Gas PipingM - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Micrography of a transverse section of the seamless pipe, presenting a ferritic-pearlitic structure.
70
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography showing the cracking starting point, in the pipe, exactly at the margin of the weld.
292
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Margin of the Weld Crack
Micrographic detail of the cracking starting point, in the pipe, exactly at the margin of the weld.
33
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Fatigue Crack
Micrography of a section tranverse to the pipe and to the weld between the 8"pipe and the 2" fitting weldolet. The crack starts exactly at the margin of the weld and propagates in the pipe longitudinal direction, in a straight line until it reaches the condition of overloading and through wall final rupture, with strong plastic deformation as can be seen around the crack.
25
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Plastic Deformation
Micrographic detail of the final fracture by overloading after the fatigue crack propagated almost through the wall thickness. The microstructure presents strong plastic deformation around the crack, in a ferritic pearlitic structure.
29
VIEW
ML00149 / Dec.2018
Vibration Induced Fatigue in a Gas Piping
M - Low Carbon SteelP - Piping spoolAp - FPSOCd - Vibration Induced Fatigue
Cm - Nital Etched Micrography by OMDf - Ductile Fracture
ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
92
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the high strenght steel microstructure, bainitic martensitic.
85
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the zinc layer at the surface.
88
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer
Micrography of the section transverse to the fracture (top of the figure). The fracture is intergranular, there are several secondary cracks, and there are deposits of zinc over the fracture. The zinc makes difficult the etch with Nital to reveal the microstructure close to the fracture surface.
67
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture
Micrographic detail of the section transverse to the fracture (top of the figure), suggesting the intergranular morphology (at the previous austenite grain boundaries) and the deposits of zinc over the fracture that create a condition of protection of the base metal during the metallographic etch, and the material is not fully etched.
60
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer

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ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrography of a stud longitudinal section in the first thread fillet adjacent to the fracture, presenting a large secondary crack without any deformation evidence. This reveals a brittle material behavior, although the hardness measured at the stud end revealed 33HRc, as should be expected by the material specification.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks

+8 more from this case →

ML00131 — Brittle Failure of a Soft Roller BearingM - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Micrographic detail of the roller bearing microstructure, close to the external surface, presenting 64 HRc and a microstructure that is martensitic with large carbides.
86
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the roller bearing microstructure, close to the external surface, presenting 64 HRc and a microstructure that is martensitic with large carbides, several presenting internal cracks.
82
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Cracks
Micrography of an axial section of the roller bearing, at the internal surface, where the hardness level was about 21 HRc, indicating that in this region the material was not properly quenched and tempered.
75
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrographic detail of the roller bearing microstructure, close to the internal surface, presenting 21 HRc that reveals that the matrix is not martensitic. It is ferritic with large aligned carbides (cracked).
72
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite
Micrographic detail of the roller bearing microstructure, close to the internal surface, presenting 21 HRc and a microstructure that is ferritic with large carbides (cracked) and small round carbides.
63
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Cracks

+5 more from this case →

ML00130 — Fatigue Fracture of Overloaded BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section. The bolt was quenched and tempered to 30HRc and presented a martensitic structure.
124
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrographic detail of the rolled thread that was heat treated later. The bolt was quenched and tempered to 30 HRc and presented a martensitic structure.
111
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
103
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
115
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface

+3 more from this case →

ML00128 — MIC of a Stored Hydraulic CylinderM - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Micrographic detail of the longitudinal section of the cylinder, at the surface, in a region where the Cr layer is detaching.
56
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Corrosion
Micrographic aspect of the longitudinal section of the cylinder steel substrate, presenting a ferritic-pearlitic structure.
207
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic-pearlitic structure of the cylinder steel substrate.
41
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrography of the longitudinal section of the cylinder , at the surface, where it was not yet damaged. The steel substrate is in the bottom of the figure, the Ni layer is in the center and the Cr layer is in the top of the figure.
38
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ni layer
Micrography of the interface between the steel substrate and the first Ni layer. The Ni layer, 160 microns thick and 300HV hardness, is uniform and presents no discontinuities.
37
VIEW
ML00128 / Apr.2018
MIC of a Stored Hydraulic Cylinder
M - Low Carbon SteelP - Chromium PlatedAp - OffshoreCd - Localized Dissolution
Cm - Nital Etched Micrography by OMDf - Ni layer

+1 more from this case →

ML00127 — Hydrogen Cracks of Cadmium Plated StudsM - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the stud presenting a tempered martensite structure in the center of the thickness.
33
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrographic image of the stud thread, in the longitudinal section, showing the segregation lines of the steel cut at the thread indicating it was machined.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the stud at the thread bottom.
27
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrographic detail of the thread top, showing that the thread was machined.
29
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Micrography of the longitudinal section of the stud showing a crack from the thread fillet, of a ductile aspect, opened during torque.
30
VIEW
ML00127 / May.2018
Hydrogen Cracks of Cadmium Plated Studs
M - Low Alloy Medium Carbon QTP - Allen StudAp - Oil and GasCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture

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ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the bolt at the bottom of the thread fillet, showing the uniform martensitic structure, not strain hardened.
90
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Uniform Structure
Micrography of the longitudinal section of the bolt at the top of the thread fillet, showing a small circunferential cracking typically of a rolling process to manufacture the thread. The thread presented no evidences of plastic deformation suggesting that the heat treatment was applied later. It is important to mention that this cracking presented no influence in the fracture of the bolt.
101
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Rolled Thread
Micrography of the longitudinal section of the bolt in the center of the thickness (ND 5/8") showing a uniform martensitic structure.
67
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the martensitic structure, uniform in the longitudinal section of the bolt, in the center of the thickness (ND 5/8"). The hardness values of the bolts varied from 39 to 41 HRc.
63
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography, after NItal etching, of the longitudinal section of the bolt, at the fracture (top of the figure), starting from the bottom of the thread (to the left side of the figure). The presence of the coating at the bolt surface shows that the fracture occurred without corrosion.
56
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture

+2 more from this case →