Kalling Etched Micrography by OM

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrography of a transverse section of the ring presenting a uniform tempered martensite structure.
43
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The longitudinal section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg). Previous austenite grains are elongated.
55
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the pipe longitudinal base metal.
148
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Micrography of the nut in the longitudinal direction, in the center of the thickness, presenting a granular austenitic structure free from detrimental phases.
475
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - In the Center of the Thickness
Original casting base metal presenting a coarse martensitic structure with a small amount of delta ferrite.
50
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side

More from these cases

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface.
27
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack
Micrographic detail of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface. it is possible to identify dissolution of the structure adjacent to the grain boundaries,
24
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrograph showing a fine acicular martensitic matrix with a branching crack network, more extensive near the right edge.
25
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack
Micrography of a transverse section of the ring, in the center, where the cracking was closed. The cracks are intergranular and not opened to the surface.
29
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Crack

+1 more from this case →

ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, close to the surface (ND 1/2"). The grain size is higher than the center of the bolt.
28
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the conector, at the fracture position, showing secondary cracks from the fracture surface.
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
The micrographic detail of the longitudinal section at the fracture surface shows intergranular morphology for the secondary cracks (longitudinal to the forging axis).
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks.
54
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks. There is a large amount of delta phase precipitated intergranular and intragranluar.
48
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
ML00076 — Hydrogen Cracking of a 17-7 PH Subsea SpringM - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the strain hardened aged martensitic structure. Small aligned delta ferrite islands can be seen.
51
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
The transverse section of the spring wire shows a strain hardened martensitic structure, aged to high strength (602 HV 0.3kg).
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrographic detail of the strain hardened aged martensitic structure.
48
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Transverse Section
Micrographic detail of a longitudinal section of the wire, at the fracture surface (top of the figure) evidencing the intergranular and transgranular aspects of the hydrogen assisted cracking mechanism. The Kalling etch does not reveal the delta ferrite. Compare with the electrolytic oxalic acid etch in the other figure.
29
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
Micrographic detail of the spring wire surface, far from the fracture, showing several small intergranular cracks.
40
VIEW
ML00076 / Jun.2017
Hydrogen Cracking of a 17-7 PH Subsea Spring
M - Precipitation Hardened Stainless SteelP - WireAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - At the Surface
ML00065 — Erosion Corrosion of Monel PipingM - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Micrographic detail of the pipe base metal presenting a granular microstructure. Some inclusions are also visible.
142
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Micrography of the elbow base metal. The comparison with the pipe micrography shows an important difference of thickness.
132
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Elbow base metal micrographic detail presenting a granular microstructure. Like the pipe, the microstructure reveals inclusions.
106
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Micrography of the pipe heat affected zone. The weld metal is on the right.
91
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side
Micrographic detail of the pipe fusion line. The pipe heat affected zone is at the bottom and the weld metal is at the top.
86
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side

+11 more from this case →

ML00062 — Inconel 718 Lock Nut with Polymer InsertM - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Micrography of the nut in the longitudinal direction, at the thread, presenting a granular austenitic structure free from detrimental phases or cold forming effects.
56
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Micrographic detail of the nut at the thread, presenting a granular austenitic structure free from cold forming effects.
52
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
Micrography of the nut in the longitudinal direction, at the Nylon insert position, showing a cold formed region at the end of the nut, with high hardness levels (about 600 HV100g).
53
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened
Micrographic detail of the nut at the cold formed region where the nut was bent over the Nylon insert. It is possible to see strain hardened structures (600HV 100g).
41
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened
ML00055 — CA6NM Blade Remanufactured by WeldingM - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Inserted casting base metal presenting a coarse martensitic structure with a small amount of delta ferrite.
24
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Micrography of the original casting blade at the fusion line of the welding with the insert casting. There is a refinement effect on the coarse base metal structure.
24
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Left Side
Micrographic detail of the fusion line of the original casting blade welded to the insert casting. There is a refinement effect on the coarse base metal structure.
21
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Left Side
Micrography of the inserted casting at the heat affected zone of the welding with the original casting. There is a refinement effect on the coarse base metal structure.
20
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Right Side
Micrographic detail of the fusion line of the inserted casting welded to the original casting. There is a refinement effect on the coarse base metal structure.
15
VIEW
ML00055 / Apr.2017
CA6NM Blade Remanufactured by Welding
M - Martensitic Stainless SteelP - Remanufacture by WeldingAp - EnergyCd - Removed From Service
Cm - Kalling Etched Micrography by OMDf - HAZ Right Side

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