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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Aspect of the stub end, that is used in combination with a lap joint flange. In this case it was prepared from a seam welded pipe, longitudinal, also with circunferential weld to the stub face (which means it was not flared). The cracking is circunferential in the non painted region, not associated to any welded area.
435
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
Aspect of a flared tubing, cold deformed at 37°, and the circumferential cracking.
483
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - General View
Macrography of a ring transverse section presenting a large variation in the grain size, revealing the diferences in the solidification rate.
453
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O solution Etched MacroDf - Casting Structure
Aspect "as received" of the seamless tube at the curved position, showing the longitudinal crack and corrosion products at the tube surface.
836
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - General View
As received aspect of the sacrificial casting, 2" internal diameter. The casting was solution annealed heat treated.
488
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Aspect Before AnalysisDf - General View
Concrete steel strand general view, presenting fracture of several wires and a corroded aspect. The full part is composed by 19 strands, each strand using 7 wires, and each wire about 5 mm diameter.
834
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
The coasters present a handmake look. The grooves are of different sizes and the octogonal shape is irregular. The pieces presented a weight that suggested that the bright finish is a metallic coating, later identified by EDS analysis as silver coating, typical of a decorative plating.
452
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Aspect Before AnalysisDf - General View
Polished cross-section showing rounded graphite nodules within a ferritic matrix, bordered by an irregular oxidized region at the surface edge.
910
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Oxide Layer

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ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Detail of the external side of the stub end showing that the cracking is circunferential, located in a corroded surface, that corresponds to the confined region under the flange.
85
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Aspect Before AnalysisDf - Cracking
The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Macrographic detail of the longitudinal section of the stub end, showing the external side to the top and the internal side to the bottom. There are multiple cracks starting from the external side.
54
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Longitudinal Section AspectDf - Multiple cracks

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ML00167 — Fatigue of a Flared Tubing ConnectionM - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Same flared tubing, with a circumferential crack, with the focus at the internal side.
65
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Aspect Before AnalysisDf - General View
Micrography of a longitudinal section of the tubing showing a granular structure, austenitic.
52
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrography of a longitudinal section of the tubing, showing the austenitic structure free from strain hardening and free from grain boundary carbides.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure, free from strain hardening and free from grain boundary carbides.
54
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Low magnification fractography by scanning electron microscopy, after a complete opening of the crack. At this magnification no micromechanism is evident.
51
VIEW
ML00167 / Aug.2020
Fatigue of a Flared Tubing Connection
M - Austenitic Stainless SteelP - TubingAp - EngineCd - Mechanical Fatigue
Cm - Fractography by SEMDf - Fracture

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ML00166 — Tin Bronze Wear Ring of Seawater PumpM - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Low magnification micrography of a transverse section of the ring showing a dendritic structure.
64
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with segregation at interdendritic regions. This structure is in a region close to the ring surface.
52
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrography of a transverse section of the ring showing a cored alpha structure with strong segregation at interdendritic regions, and regions of a white structure at grain boundaries. This structure is in a region close to the center of the ring.
51
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Dendritic
Micrographic detail of the cored alpha structure with light segregation at intergranular regions (light layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the ring surface, where the solidification was quicker.
49
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics
Micrographic detail of the cored alpha structure with strong segregation at intergranular regions (dark layer at grain boundaries), and a white euctetoid structure (alpha and delta) at interdendritic space. This structure is in a region close to the center of the ring, where the solidification was slower.
47
VIEW
ML00166 / Jul.2020
Tin Bronze Wear Ring of Seawater Pump
M - Tin BronzeP - Wear RingAp - ShipCd - Removed From Service
Cm - FeCl3+HCl+H2O Etched MicroDf - Grain boundary intermetallics

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ML00165 — SCC of Aluminum Bronze Heating CoilM - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Aspect of the external tube surface after cleaning. It is possible to see that the cracks are longitudinal to the tube and localized in positions where the surface is corroded.
132
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - External Surface
Aspect of the internal tube surface after a longitudinal cut, without cleaning. It is possible to see a clean surface inside the tube.
104
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - Surface AspectDf - Internal Surface
Micrography of the tranverse section of the tube, in the center of the thickness. There are small grains and large grains, characterizing a dual grain size. The large grains size is about 100 microns, more than 10 times larger than the average size of the smaller grains size.
101
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Dual grain sizes
Micrographic detail of the alpha microstructure presenting dual grain sizes. Two different types of twins are presented in the structure: annealing twins and deformation twins, suggesting that the material was probably partially recristalized after cold deformation and stress relief treatment.
87
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - FeCl3+HCl+H2O Etched MicroDf - Alpha
Micrography of a transverse section of the bent tube, external surface (OD) to the top and internal surface (ID) to the bottom of the figure. At the through wall cracking position, the external surface presented a layer of intergranular corrosion.
95
VIEW
ML00165 / Jul.2020
SCC of Aluminum Bronze Heating Coil
M - Aluminum BronzeP - Seamless tubeAp - Oil and GasCd - Stress Corrosion
Cm - As polished micrographyDf - Cracking

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ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Macrography of a longitudinal section of the valve body, presenting the granular structure. The main bore diameter is 2". The casting was tested in two positions. In radial direction in the center of the body (3" solid), and in the longitudinal direction in the wall (1" thick).
78
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Macro Oxalic Acid Electrolytic EtchedDf - Longitudinal Section
Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

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ML00155 — Failure of a Prestressed Concrete Steel StrandM - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
General aspect of the degradated wires of the strand, most part presenting rust and rupture.
107
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - General View
General aspect of the degradated wires of the strand, most part presenting rust and rupture. There are two mais aspects of the degradation: wire thickness reduction by corrosion and cracks creating a longitudinal fracture of several wires.
96
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - Aspect Before AnalysisDf - Fracture
Micrography of a wire in a longitudinal section, presenting a predominantly oearlitic structure, highly strained. The wires did not present any coating.
104
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Higher magnification detail of the predominantly pearlitic microstructure of the wire.
88
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Predominantly Pearlitic
Macrography of a typical corroded wire in a longitudinal section, showing loss of thickness by corrosion.
75
VIEW
ML00155 / Jan.2020
Failure of a Prestressed Concrete Steel Strand
M - High Carbon SteelP - Wire RopeAp - StructureCd - Corrosion Fatigue
Cm - NItal Etched MacroDf - Corrosion

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ML00156 — Antique Silver Plated Decorative PieceM - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Piece that was analysed by non destructive tests. Octogonal shape. Two irregular grooves. The coaster was manufactured in a cooper alloy substrate and a metallic coating. The analysis to reveal the substrate microstructure was conducted on the back of the part, in a non destructive preparation, that included light grinding, polishing and etching.
61
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Aspect Before AnalysisDf - General View
Light grinding the back of the coaster. The surface was only partially ground, removing the metallic coating, and exposing the substrate, that appeared yellow indicating the manufacturing in a cooper alloy.
63
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Preparation TechniqueDf - General View
Aspect of the back of the coaster after grinding. The coating was partially removed. The chemical analysis was conducted in the ground part to obtain the composition of the substrate, that showed to be a yellow brass alloy. It is interesting to note that the alloy presented 2.3% lead.
63
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Preparation TechniqueDf - At the Surface
Back of the coaster showing the region that was prepared for the non destructive analysis. It was ground and polished (the coating was removed), showing the yellow aspect of the substrate, in the left bottom part of the image.
64
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - As polishedDf - General View
Image presenting the back of the coaster where the microstructure of the substrate was identified. The composition of the brass (about 35% Zn) indicates that the expected structure is alpha plus beta. The front of the coaster presents two grooves which surface morphology was analyzed by scanning electron microscopy.
65
VIEW
ML00156 / Jan.2020
Antique Silver Plated Decorative Piece
M - BrassP - Decorative PieceAp - OrnamentalCd - Non Destructive Examination
Cm - Surface AspectDf - General View

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ML00001 — Thermal Fatigue of Cast IronM - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Flat casting product presenting several thermal fatigue cracks all thorugh the surfaces. 1" thicknes.
171
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - Transverse Section AspectDf - Cracks Transverse to the Surface
Detail of figure 2, showing multiple fatigue cracks due to thermal cycles.
136
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - NItal Etched MacroDf - Cracks Transverse to the Surface
The 1" flat casting product presents a ferritic perlitic matrix and graphite nodules.
112
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Graphite in Nodules
Center of the flat casting product, presenting nodular graphite and ferritic perlitic matrix.
113
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Predominantly Ferritic Matrix
Nodular cast iron presenting a ferritic perlitic matrix.
109
VIEW
ML00001 / Dec.2017
Thermal Fatigue of Cast Iron
M - Nodular Cast IronP - CastAp - SiderurgyCd - Thermal Fatigue
Cm - Nital Etched Micrography by OMDf - Matrix of ferrite and pearlite

+4 more from this case →