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Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Granular Capture method: Optical Microscope clear all

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Micrography of the fork handle in the transverse section, curved, presenting differences between grain size and morphology. In the middle section there are elongated grains and close to the surfaces there are smaller and more equiaxed grains.
81
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Transverse Section
Micrography of the plate in a section, in the middle of the thickness. The aligned pitting is associated to the chemical etch of inclusions and second phases. The structure is granular but the grain boundaries do not appear at that magnification, originally 50x.
50
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
76
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section
Image by scanning electron microscopy of the metallurgically bonded interface of the internally cladded pipe. It is a longitudinal seam welded pipe, with substrate in low alloy steel X65 and clad plate in Alloy 625 (welded by a solid state process). The region is a detail in the side of the Ni alloy clad plate where a grain refinement has occurred probably due to recrystallization of a strain hardened region during later heat treatment. The microhardness of this region is a lot higher than the value obtained out of this region, in the clad plate.
904
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Oxalic Acid Electrolytic EtchDf - Clad Interface
Micrography of the welded joint, at the root, presenting hot cracks. The imposed high energy in the root due to the ceramic backing support created a condition for cracking.
1100
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Hot cracking
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrography of the longitudinal section of the forging material, presenting a granular austenite, precipitation hardened.
84
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Longitudinal Section
Micrography of the pipe longitudinal base metal.
148
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side

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ML00151 — Ferritic Stainless Steel of a Flatware ForkM - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Micrography of the fork handle in the center of the transverse section, curved, presenting larger ferritic grains with elongated morphology.
70
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure
Micrographic detail of the ferritic grains with elongated morphology in the center of the transverse section, curved.
58
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Ferrite
The micrography as polished in the transverse section shows a small amount of inclusions in the steel.
62
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Detail of the non metallic inclusions in the steel. The yellow and black colours and morphologies suggest Ti base and oxides.
65
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Micrography of a longitudinal section of the fork, at the scoop to handle position (scoop to the right of the figure and handle to the left). The full thickness is presented in the image and it is possible to see that in the handle location the ferritic grains are larger in the center of the thickness than close to the surfaces, and in the scoop position the grains tend to be more uniform through the thickness.
50
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Longitudinal Section

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ML00145 — Impact of a .380 Winchester on 6061 T6 PlateM - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Micrography of the plate in a section, in the middle of the thickness, in a position where the plate was not affected by the shot. The microstructure is granular although the grain boundaries are not resolvable at this magnification. The black spots are localized corrosion in aligned particles.
49
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Aligned particles
Micrographic detail of the plate in the middle of the thickness. At this magnification it is possible to see the grain boundaries and the black spots are localized etching in aligned particles.
43
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Granular structure
Micrographic detail of the plate in the middle of the thickness. At this magnification it is possible to see the grain boundaries and the black spots are localized etching in aligned particles.
37
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Granular structure
Micrography of the damaged plate at the side of the bullet impact, top of the figure. The perforated hole expulsed the material to the top and bottom directions. There are evidences of plastic deformation of the plate microstructure and the hardness level close to the hole increased from 123 HV to 131 HV (1kg)
17
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Strain Hardened
Micrography of the damaged plate at the side of the bullet impact, top of the figure. The perforated hole expulsed the material to the top and bottom directions and the microstructure shows plastic deformation.
16
VIEW
ML00145 / Sep.2018
Impact of a .380 Winchester on 6061 T6 Plate
M - Aluminum Magnesium SiliconP - Rolled PlateAp - StructureCd - Pierced
Cm - Keller Etched Micrography by OMDf - Plastic Deformation

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ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
64
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section
Micrographic detail of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
61
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked. The material presented 38HRc hardness.
57
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked.
62
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrographic detail of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked.
59
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

+6 more from this case →

ML00133 — Seam Welded Pipe Cladded with Alloy 625M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Micrography of a longitudinal section of the pipe substrate, in low magnification, showing a uniform microstructure,
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Base Metal
Micrography of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure obtained by the pipe quenching and tempering,
48
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Micrographic detail of a longitudinal section of the pipe substrate showing a uniform bainitic microstructure,
50
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Bainite
Micrography of a longitudinal section of the pipe at the interface with the clad plate, with Nital etch that reveals only the low alloy steel structure, to the left side of the image.
55
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Clad Interface
Micrography of a longitudinal section of the pipe at the interface with the clad plate, with Nital etch that reveals only the low alloy steel structure, to the left side of the image.
51
VIEW
ML00133 / May.2018
Seam Welded Pipe Cladded with Alloy 625
M - LAS / Ni AlloyP - Longitudinal Seam Welded PipeAp - Oil and GasCd - Welding
Cm - Nital Etched Micrography by OMDf - Clad Interface

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ML00118 — Non qualified GMAW of Aluminum PlatesM - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Micrography of the welded joint, at the root, showing hot cracks with intergranular morphology.
146
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Hot cracking
Micrographic detail of the welded joint, at the root, presenting hot cracks. The presence of these defects were responsible for reducing the material strenght (rupturing in lower strenght than the requirements) and ductility (cracking in bending tests).
116
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Hot cracking
Low magnification micrography of the plate base metal, presenting granular structure not clearly identified and aligned particles.
88
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Base Metal
Micrography of the plate base metal, presenting granular structure evidenced by the different shadows in the grains.
76
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Base Metal
Micrographic detail of the aligned particles in the plate base metal. The grain boundaries are not clearly identified in this higher magnification.
73
VIEW
ML00118 / Jan.2018
Non qualified GMAW of Aluminum Plates
M - Aluminum Magnesium ManganeseP - Welded Testpiece for QualificationAp - ShipCd - Non qualified
Cm - Keller Etched Micrography by OMDf - Base Metal

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ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The micrography of a longitudinal section of the bolt close to the surface, at the thread, shows that it was machined from a bar, not rolled.
37
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Machined Thread
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, close to the surface (ND 1/2"). The grain size is higher than the center of the bolt.
28
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00078 — Hydrogen Cracking of IN 718 Subsea ConnectorM - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Micrography of the longitudinal section of the conector, at the fracture position, showing secondary cracks from the fracture surface.
63
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
The micrographic detail of the longitudinal section at the fracture surface shows intergranular morphology for the secondary cracks (longitudinal to the forging axis).
64
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks.
54
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of a longitudinal section of the connector, at the fracture surface (in the top), showing intergranular secondary cracks. There is a large amount of delta phase precipitated intergranular and intragranluar.
48
VIEW
ML00078 / Jun.2017
Hydrogen Cracking of IN 718 Subsea Connector
M - NiCrFe AlloyP - ForgingAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
ML00065 — Erosion Corrosion of Monel PipingM - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Micrographic detail of the pipe base metal presenting a granular microstructure. Some inclusions are also visible.
142
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Micrography of the elbow base metal. The comparison with the pipe micrography shows an important difference of thickness.
132
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Elbow base metal micrographic detail presenting a granular microstructure. Like the pipe, the microstructure reveals inclusions.
106
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Micrography of the pipe heat affected zone. The weld metal is on the right.
91
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side
Micrographic detail of the pipe fusion line. The pipe heat affected zone is at the bottom and the weld metal is at the top.
86
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side

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