Detrimental phases

4 cases · 55 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of the pipe base metal presenting a refined duplex ferritic austenitc structure, banded.
47
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Macrography transverse to the circunferential weld, longitudinal to the piping, presenting the location, a little far from the welded joint margin, where the through wall cracking is positioned.
160
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Through Wall Cracking

More from these cases

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrography of a longitudinal section of the sleeve close to the external surface, evidencing a tugnsten carbide thermal spray layer, thickness about 0.2 mm, at the sleeve outer diameter (OD), black due to the etch (top of the figure). This WC layer was deposited over a stainless steel layer disposed in several layers, non etched.
42
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrographic detail of the interface between the two thermal spray layers, the first one in stainless steel (bottom of the figure) and the second one, at the surface,in tungsten carbide (top of the figure). The micrographic sample is etched and that is why the WC is dark (black) and the stainless steel is light (non etched).
41
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Thermal Spray Layer
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface
Micrographic detail of the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma at the delta and gamma interface. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of the longitudinal section of the cast sleeve in the middle of the thickness. The microstructure is coarse, austenitic ferritic.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - In the Center of the Thickness

+12 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite

+8 more from this case →

ML00049 — Pipe to Flange Welded Joint in a 14" ND Superduplex SpoolM - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Micrographic detail of the pipe base metal presenting a refined duplex ferritic austenitc structure, banded.
55
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Base Metal
Micrographic detail of the pipe base metal presenting a refined duplex ferritic austenitc structure, banded.
56
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrography of the flange base metal presenting a coarse duplex ferritic austenitc structure.
88
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrographic detail of the flange base metal presenting a coarse duplex ferritic austenitc structure. Detrimental phases associated to the ferritic structure.
62
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrography of the pipe heat affected zone. In the left the pipe base metal, with banded duplex structure; and in the right the weld metal, with Widmanstatten morphology of the structure.
43
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone

+11 more from this case →

ML00002 — Preferential Dissolution and Cracks in SDSSM - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Longitudinal section micrography at the cracked position, close to the external surface of the flange, showing cracks transverse to the thickness, associated to the microstructure.
147
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Cracks Transverse to the Surface
Longitudinal section micrography at the cracked position, close to the internal surface of the flange (exposed to the corrosive fluid), showing preferential dissolution associated to the microstructure.
133
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Preferential Dissolution
Micrography of the flange in the longitudinal section. The flange microstructure is ferritic austenitic, presenting a coarse structure.
102
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Coarse Structure
Micrographic detail of the flange microstructure in the longitudinal section. The flange is ferritic austenitic, presenting 70% of austenite. In the ferrite network there are evidences of precipitation/formation of detrimental phases.
113
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure
Micrographic detail of the flange microstructure in the longitudinal section. The flange is ferritic austenitic, presenting 70% of austenite. In the ferrite network there are evidences of precipitation/formation of detrimental phases.
100
VIEW
ML00002 / Jan.2018
Preferential Dissolution and Cracks in SDSS
M - Super Duplex Stainless SteelP - Fabrication WeldAp - PipingCd - Preferential Dissolution
Cm - NaOH Electrolytic Etched MicroDf - Duplex structure