Optical Microscope

7 cases · 47 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Microstructure: Duplex Ferritic Austenitic Detail focus: Sampling and Analysis clear all

Optical Microscope — sub-branches

NaOH Electrolytic Etched Micro 47

Results

SortNewestOldestTitle A-ZTitle Z-A
Micrography of the heat affected zone of the pipe to the fitting, at the pipe position, where the weld is in angle to the pipe (welded at the pipe surface). Weld metal to the top.
85
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of a longitudinal section of the sleeve, at the external surface where there are two layers of coating. The electrolytic etch evidenced the duplex stainless steel substrate (bottom of the figure) and the weave interface of the substrate and the first thermal spray layer, about 1 mm thick, in a stainless steel. The surface layer, of tugnsten carbide, about 0.2 mm thick, is black and not clearly visible in this figure.
50
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - External Surface
Low magnification micrography of the valve at the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
47
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Welded Joint
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of the tubing fusion line. The welding was conducted in two passes. The average hardness at the heat affected zone of the tubing is 257 HV5.
825
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Fusion Line Left Side
Micrography of a transverse section of the fitting, at the cracking position. Note the through wall cracking at the coarse austenitic ferritic structure.
43
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrographic detail of the pipe base metal presenting a refined duplex ferritic austenitc structure, banded.
55
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Base Metal

More from these cases

ML00150 — Vibration Induced Fatigue in a SS Oil PipingM - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Micrography of the heat affected zone of the pipe to the fitting, at the pipe position. Base metal to the bottom of the figure and fusion line to the top.
87
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the heat affected zone (HAZ) of the pipe. The amount of ferrite in the HAZ is a little higher than in the pipe base metal.
86
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the heat affected zone of the pipe to the fitting, at the fitting position. The fitting is welded in the thickness. The fusion line is in the bottom of the figure.
74
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the heat affected zone (HAZ) of the fitting, welded to the pipe. The forged fitting base metal is to the top of the figure and the fusion line is to the bottom.
71
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the heat affected zone (HAZ) of the fitting. The amount of ferrite in the HAZ is a little higher than in the pipe base metal.
70
VIEW
ML00150 / Dec.2018
Vibration Induced Fatigue in a SS Oil Piping
M - Duplex Stainless SteelP - PipingAp - FPSOCd - Vibration Induced Fatigue
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone

+4 more from this case →

ML00147 — WC Layer Detached from a Cast Lean DuplexM - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Micrography of the longitudinal section of the sleeve, at the interface between the substrate and the first thermal spray layer. The substrate (bottom of the figure) shows a ferritic-austenitic microstructure and detrimental phases that look like sigma. The thermal spray layer (top of the figure) presents the non-etched stainless steel, disposed in layers, with oxides (gray) and voids (black). The substrate is deformed in a thin layer at the interface.
38
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Close to the External Surface
Micrography of the longitudinal section of the cast sleeve in the middle of the thickness. The microstructure is coarse, austenitic ferritic.
34
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - In the Center of the Thickness
Micrography of the longitudinal section of the cast sleeve, close to the internal diameter (ID). The microstructure is coarse, austenitic ferritic, and presents the same microstructure, ferritic and austenitic, all through the thickness.
21
VIEW
ML00147 / Aug.2018
WC Layer Detached from a Cast Lean Duplex
M - Lean Duplex Stainless SteelP - Centrifugal CastingAp - ShipCd - Lack of Sealing
Cm - NaOH Electrolytic Etched MicroDf - Internal Surface
ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrography of the valve at the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
46
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrographic detail of the fusion line of the welded joint of the body to the insert (fillet weld). The cracking was arrested at the position of this welded joint because the structures of the weld metal, insert and heat affected zones are tough (austenitic in the weld metal and insert, and free from sigma in the HAZ) .
39
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the valve at the welded joint of the body to the insert (fillet weld). The heat affected zone shows that the sigma phase was removed, which means that the base metal was degradated and during welding the thermal cycle created a condition to remove the sigma phase (dissolve it).
38
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrographic detail of the heat affected zone of the valve to the insert joint showing that the sigma phase was removed, which means that the base metal was degradated and during welding the thermal cycle created a condition to dissolve the sigma phase.
39
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
ML00100 — Superduplex Tubing to Forging Welded JointM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Micrography of the tubing heat affected zone.
69
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - HAZ Left Side
Micrography of the tubing heat affected zone.
68
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - HAZ Left Side
Low magnification micrography of the superduplex stainless steel tubing (base metal), in the longitudinal direction. Refined ferritic-austenitic structure. The average hardness in the section is 264HV5.
58
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Base Metal Left Side
Micrography at the center of the weld metal, showing the interface between the two passes. The average hardness of the weld metal is 260 HV5.
49
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Weld Metal in the Center
Micrography at the center of the weld metal.
41
VIEW
ML00100 / Nov.2017
Superduplex Tubing to Forging Welded Joint
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Welding
Cm - NaOH Electrolytic Etched MicroDf - Weld Metal

+6 more from this case →

ML00049 — Pipe to Flange Welded Joint in a 14" ND Superduplex SpoolM - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Micrography of the pipe heat affected zone. In the left the pipe base metal, with banded duplex structure; and in the right the weld metal, with Widmanstatten morphology of the structure.
43
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Higher magnification of the pipe heat affected zone. The amount of ferrite increases with the proximity of the fusion line (to the right).
38
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the flange heat affected zone. In the right the flange base metal, with coarse structure and detrimental phases associated to the ferrite; and in the left the weld metal, with Widmanstatten morphology of the structure.
36
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Higher magnification of the flange heat affected zone. The detrimental phases in the ferrite structure is clearly being dissolved with the proximity of the fusion line (to the left).
28
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Heat Affected Zone
Micrography of the root weld metal. Duplex ferritic austenitic structure with Widmanstatten morphology.
30
VIEW
ML00049 / Apr.2017
Pipe to Flange Welded Joint in a 14" ND Superduplex Spool
M - Super Duplex Stainless SteelP - Piping spoolAp - Oil and GasCd - Removed From Service
Cm - NaOH Electrolytic Etched MicroDf - Weld Metal in the Root

+5 more from this case →