Optical Microscope

35 cases · 135 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Standard: AISI Detail focus: Microstructure clear all

Optical Microscope — sub-branches

As polished micrography 6Eletrolytically Etched Micrography by OM 2Kalling Etched Micrography by OM 5Micro by OM, HCl + Ethanol + Picric Acid 6Micrography by OM 2Micrography by OM using A262 Method A 15NaOH Electrolytic Etched Micro 3Nital Etched Micrography by OM 80Oxalic Acid Electrolytic Etch 16

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Tempered martensite of the pipe body of this API 5D grade S135 drill pipe. The material presents, at this low magnification micrographic aspect, a slightly banded structure, usual for this type of drill pipe.
58
VIEW
ML00159 / Mar.2020
Collapse of a Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Ductile Behavior
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrography of the wheel in the center of the thickness, presenting a predominantly pearlitic structure and average hardness abot 196HB.
74
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
The coarse structure in the center of the shaft thickness is evidenced by free ferrite islands at the previous austenite grains. The presence of a pearlitic structure evidences the slow cool of the material.
85
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrography of the fork handle in the center of the transverse section, curved, presenting larger ferritic grains with elongated morphology.
70
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure
Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the roller bearing microstructure, close to the external surface, presenting 64 HRc and a microstructure that is martensitic with large carbides.
86
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the weld metal with islands of a coarse ferritic structure, degradated (recristalized) from an acicular morphology during to the long heat treatment cycle in high temperature. The post welding heat treatment (PWHT) was conducted during 12 hours at 640°C.
700
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Coarse Structure

More from these cases

ML00159 — Collapse of a Drill PipeM - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Ductile Behavior
Micrographic detail of the tempered martensite in the longitudinal section of the pipe body. Uniform structure.
45
VIEW
ML00159 / Mar.2020
Collapse of a Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Ductile Behavior
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the tempered martensite in the longitudinal section of the pipe body.
39
VIEW
ML00159 / Mar.2020
Collapse of a Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Ductile Behavior
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of sheared pipe, showing strong plastic deformation at the fracture. The structure shows the shear effect at the fracture.
16
VIEW
ML00159 / Mar.2020
Collapse of a Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - O&G Well DrillingCd - Ductile Behavior
Cm - Nital Etched Micrography by OMDf - Martensite
ML00158 — Surface Hardened Carbon Steel WheelM - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Micrographic detail of the coarse pearlitic structure in the center of the wheel thickness. The part presents a wrought structure.
73
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrographic detail of the tempered martensitic structure.
50
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic aspect of the pearlitic structure at the surface not heat treated, showing a lower grain size than in the center of the thickness.
35
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrographic detail of the pearlitic microstructure in a region where the structure is not so coarse than in the center of the thickness.
30
VIEW
ML00158 / Feb.2020
Surface Hardened Carbon Steel Wheel
M - High Carbon SteelP - WheelAp - TransportationCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides, strain hardened. The hardness values of the material are from 200HV1 to 300HV1, that meets the class 2 of strenght (ASTM A193 B8M class 2).
79
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
ML00152 — Low Alloy Steel Pump ShaftM - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
The longitudinal section of the shaft, at the surface, presenting only a small refining in the previous austenite grain boundaries than in the center, indicating that the material was slowed colled from forming and not heat treated.
67
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Coarse Structure
Micrographic detail of the pearlitic structure at the surface of the shaft thickness.
69
VIEW
ML00152 / Dec.2018
Low Alloy Steel Pump Shaft
M - High Strength Low AlloyP - ShaftAp - Oil and GasCd - Removed From Service
Cm - Nital Etched Micrography by OMDf - Pearlite
ML00151 — Ferritic Stainless Steel of a Flatware ForkM - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Micrographic detail of the ferritic grains with elongated morphology in the center of the transverse section, curved.
58
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Ferrite
The micrography as polished in the transverse section shows a small amount of inclusions in the steel.
62
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Detail of the non metallic inclusions in the steel. The yellow and black colours and morphologies suggest Ti base and oxides.
65
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - As polished micrographyDf - Non Metallic Inclusions
Micrography of a fork longitudinal section, in the center of the thickness, at the scoop position. The ferritic grains are equiaxial and uniform.
49
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure
Micrography of a fork handle in the longitudinal section, presenting the larger ferritic grains.
45
VIEW
ML00151 / Dec.2018
Ferritic Stainless Steel of a Flatware Fork
M - Ferritic Stainless SteelP - Foodstuff ArticleAp - KitchenCd - Typical manufacturing
Cm - Micro by OM, HCl + Ethanol + Picric AcidDf - Granular structure

+2 more from this case →

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
ML00131 — Brittle Failure of a Soft Roller BearingM - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Micrographic detail of the roller bearing microstructure, close to the internal surface, presenting 21 HRc that reveals that the matrix is not martensitic. It is ferritic with large aligned carbides (cracked).
72
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite
Ferritic structure close to the internal diameter of the cylindrical roller bearing, in the circuferemtial direction, presenting large carbides (not aligned due to the direction of the section) and small round carbides. in this region the fracture presented ductile micromechanisms (dimples) as well as decohesion of large carbides and cleavage facets, typical of overloading of this low toughness material.
52
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Ferrite
Martensitic structure close to the external diameter of the cylindrical roller bearing, in the circuferemtial direction, presenting large carbides (not aligned due to the direction of the section) and a martensitic matrix. in this region the fracture presented quasecleavage micromechanism as well as decohesion of large carbides.
36
VIEW
ML00131 / Apr.2018
Brittle Failure of a Soft Roller Bearing
M - Wear Resistant SteelP - Roller BearingAp - Mechanical IndustryCd - Heat Treatment Defect
Cm - Nital Etched Micrography by OMDf - Martensite
ML00129 — Non qualified WPS for High Strength SteelM - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Micrographic detail of the base metal structure, quenched and tempered martensite. The base metal adopted in the test coupon presented a hardness level of 217HB (Brinell hardness of the certificate) and after the PWHT cycle the measured base metal hardness is 224 HV10.
51
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the heat affected zone at the face of the joint, close to the fusion line. The structure is martensitic but the previous austenite grain boundary was not large. 248HV10.
47
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the weld metal at the face of the joint showing the acicular ferrite structure. The hardness level in this region is about 250HV10.
41
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Acicular Ferrite
Micrographic detail of the heat affected zone at the root of the joint, submitted to several welding reheating cycles. The structure is martensitic with a refined previous austenite structure.
38
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the weld metal at the root of the joint showing a mixture of acicular structure with equiaxial ferritic structure. The hardness level in this region is about 231HV10.
34
VIEW
ML00129 / Apr.2018
Non qualified WPS for High Strength Steel
M - Low Alloy Medium Carbon QTP - Welded Testpiece for QualificationAp - Oil and GasCd - Non qualified
Cm - Nital Etched Micrography by OMDf - Ferrite