Optical Microscope

24 cases · 43 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Detail focus: Intergranular Cracking clear all

Optical Microscope — sub-branches

As polished micrography 8FeCl3+HCl+H2O Etched Micro 1H2SO4+HNO3+H3PO4 Etched Micro 1Kalling Etched Micrography by OM 10Micrography by OM 4Micrography by OM using A262 Method A 3Nital Etched Micrography by OM 15Oxalic Acid Electrolytic Etch 1

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Micrographic detail of a longitudinal section of the stud, at the fracture surface, in the thread. It is possible to see primary precipitates (yellow) already cracked and intergranular propagation.
37
VIEW
ML00075 / Jun.2018
Hydrogen Cracking of IN 718 Subsea Fasteners
M - NiCrFe AlloyP - StudAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of intergranular cracks close to the fracture of the bolt, near the bolt surface where the macroscopi aspect was brittle.
82
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
Multiple intergranular cracks transverse to the bolt axis. Hydrogen assisted cracking due to cathodic protection of a high strenght steel. Micrography in the "as polished" condition.
472
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Intergranular Cracking
The micrographic aspect of the cracks in a section transverse to the weld (the removed sample), shows that there are cracks with different sizes, the larger are filled with products that indicate they were opened for longer times.
67
VIEW
ML00071 / Jan.2019
Reheating Cracking of a CrMo Vessel Weld
M - CrMo SteelP - In Field WeldAp - EnergyCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Micrography of the fractured region, from the superior plate side, showing that the intergranular cracking occurred at the coarse grain heat affected zone. The structure is bainitic and there are segregated regions in the previous austenite grain boundaries.
50
VIEW
ML00069 / May.2017
Liquation Cracks in SAW of Low Carbon Steel
M - Low Carbon SteelP - Fabrication WeldAp - AutomotiveCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
The cracking from the refrigeration hole presents an intergranular morphology, as shown in the micrography of a transverse section of the blade.
35
VIEW
ML00042 / Apr.2017
Gas Turbine Blade IN 939, Coated
M - NiCrCo AlloyP - CastAp - Gas TurbineCd - Intergranular Cracking
Cm - H2SO4+HNO3+H3PO4 Etched MicroDf - Intergranular Cracking
Micrography of a section transverse to the repair weld showing that the macroscopic crack, detected at the surface of the plate, occurred exactly at the margin of the weld bead. It is possible to see that the bead was deposited over a region that was already corroded (intergranular corrosion) and the macroscopic crack is the opening of several corroded grains.
158
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Cracking
Transverse section of the fitting that suffered a longitudinal cracking. As polished. The wrought fitting has suffered intergranular stress corrosion cracking from the internal surface, exposed to hot caustic environment.
566
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Micrography by OMDf - Intergranular Cracking

More from these cases

ML00074 — Hydrogen Cracking of a 17-4 PH Subsea BoltM - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
The micrography, in the "as polished" condition, of the longitudinal section of the bolt showing that there are non-continuous longitudinal cracks, intergranular, associated to regions of impurities, probably segregation bands, as evidenced by the grey elongated sulfide inclusions.
76
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Intergranular Cracking
Micrographic detail of the longitudinal cracks in the middle of the bolt, that generaate the secondary cracks that appear at the fracture surface.
79
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Intergranular Cracking
ML00073 — Hydrogen Cracking of a LAS Subsea FastenerM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Thin intergranular cracks in the center of the bolt thickness. Not continuous and not opened to the surface.
46
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
Micrographic detail of the intergranular morphology of the internal hydrogen cracks.
44
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
ML00069 — Liquation Cracks in SAW of Low Carbon SteelM - Low Carbon SteelP - Fabrication WeldAp - AutomotiveCd - Welding Defect
Micrography of the fractured region, from the weld metal side, showing that the intergranular cracking occurred at the coarse grain heat affected zone. The structure is bainitic and there are segregated regions in the previous austenite grain boundaries.
127
VIEW
ML00069 / May.2017
Liquation Cracks in SAW of Low Carbon Steel
M - Low Carbon SteelP - Fabrication WeldAp - AutomotiveCd - Welding Defect
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking
ML00015 — Intergranular Corrosion of 304SS PlateM - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Detail of the fusion line region of the repair weld. It is possible to see that the cracks are filled with oxides indicating that the material was already corroded when the bead was deposited.
128
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Cracking
Detail of the fusion line region of the repair weld. It is possible to see that the cracks are filled with oxides indicating that the material was already corroded when the bead was deposited.
108
VIEW
ML00015 / Oct.2017
Intergranular Corrosion of 304SS Plate
M - Austenitic Stainless SteelP - Rolled PlateAp - RefineryCd - Intergranular Corrosion
Cm - Micrography by OM using A262 Method ADf - Intergranular Cracking
ML00011 — Intergranular SCC of Pure NickelM - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Transverse section of the fitting that suffered a longitudinal cracking. As polished. The wrought fitting has suffered intergranular stress corrosion cracking from the internal surface, exposed to hot caustic environment.
70
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Micrography by OMDf - Intergranular Cracking