Optical Microscope

67 cases · 615 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Standard: UNS clear all

Optical Microscope — sub-branches

As polished micrography 57Chromic Acid Electrolytic Etched 1Eletrolytically Etched Micrography by OM 5FeCl3+HCl+Ethanol Etched Micro 15FeCl3+HCl+H2O Etched Micro 18Glyceregia Etched Micrography by OM 1H2SO4+HNO3+H3PO4 Etched Micro 1Kalling Etched Micrography by OM 135Keller Etched Micrography by OM 21Kroll Etched Micrography by OM 5Micrography by OM 36Micrography by OM using A262 Method A 65Micrography by OM, HF + HNO3 + H2O etch 2NaOH Electrolytic Etched Micro 49Nital Etched Micrography by OM 190Oxalic Acid Electrolytic Etch 14

Results

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The wheel microstructure changed a little depending the thickness. In the region of WHEEL 1 fracture and WHEEL 2 cracking, it presented an alpha matrix with a networklike precipitates interdendritic.
46
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched Micrography by OMDf - Hypoeutetic
Micrographic aspect of the tube out of the damaged region, in a longitudinal section, showing the grain refined copper structure.
96
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - In the Center of the Thickness
In a cut perpendicular to the macroscopic secondary crack it is possible to see several brittle microcracks (branched), indicating that an embrittlement has occurred.
22
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - As polished micrographyDf - Brittle Cracks
Low magnification micrography of a strain hardened pearlitic structure, in a longitudinal section, of one 3.2mm round wire of one strand.
62
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Aged microstructure of the HP stainless steel, modified with 1%Nb, cast fitting, tubular, operating for 6 years in a furnace which design temperature is 1100°C. The material presented a network of primary carbides, white and grey, and an austenitic matrix with coalescing secondary precipitation. Some voids. The Vickers identation indicates a hardness value about 260HV 100g in the aged austenitic matrix.
492
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Microhardness identations
Micrography of a transverse section of the spring, at the surface showing pits full of deposits.
36
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Transverse Section
Metallographic image of a longitudinal section of the clamp (axis in the vertical direction), showing a refined ferritic perlitic structure.
34
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Uniform granular microstructure of the aluminum brass, monophasic alpha.
44
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Alpha

More from these cases

ML00183 — Ductile Behavior of an Aluminum WheelM - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Detail of the alpha matrix with an eutectic networklike precipitates, interdendritic. Presence of acicular iron rich phases (dark gray).
51
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched Micrography by OMDf - Networklike precipitates
Micrography transverse to the fracture surface of the WHEEL 1. The fracture is in the up right position of the photo and it can be observed a secondary cracking following the interdendritic precipitates.
33
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched Micrography by OMDf - Radial Section
Micrographic detail of the secondary crack from the fracture surface of the WHEEL 1, following the interdendritic precipitates.
36
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched Micrography by OMDf - Fracture
Dendritic branching structure of the aluminum matrix, with fine interdendritic features visible against a darker surrounding phase.
2
VIEW
ML00183 / Dec.2022
Ductile Behavior of an Aluminum Wheel
M - Aluminum Silicon MagnesiumP - CastingAp - AutomotiveCd - Ductile Behavior
Cm - Keller Etched Micrography by OMDf - Crack
ML00180 — Local Melting of Copper Cooling TubesM - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Micrographic detail of the granular copper structure, a little far from the overheated region.
102
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - Granular structure
Micrographic detail of the granular copper structure, out of the damaged area. The dark particles are non metallic (oxides).
93
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - Granular structure
Micrographic aspect, as polished, of a transverse section of the tube (bottom side of the image, orange), at the interface between the tube and the melted steel over the external diameter (top side of the image, grey). In the copper tube there are several microcracks and regions of incipient melting (voids).
41
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - As polished micrographyDf - Cracks
Micrographic aspect of the tube wall under the localized thinning, in a transverse section, showing a coarse structure due to high temperature grain growth.
37
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - Overheating
Micrographic detail of the high temperature grain growth in the tube microstructure.
31
VIEW
ML00180 / Mar.2022
Local Melting of Copper Cooling Tubes
M - Pure CopperP - Cooling TubeAp - SiderurgyCd - Overheating
Cm - FeCl3+HCl+H2O Etched MicroDf - Coarse Structure

+6 more from this case →

ML00176 — Hydride Formation in a Titanium BladeM - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
The main crack is to the top and the blade surface is to the right, in this micrography that does not reveal any plastic deformation, with transgranular and integranular cracks.
24
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Brittle Fracture
Transgranular and integranular cracks in the alpha matrix full of acicular hydrides .
17
VIEW
ML00176 / Nov.2021
Hydride Formation in a Titanium Blade
M - Unalloyed TitaniumP - BladeAp - Oil and GasCd - Hydride Formation
Cm - Micrography by OM, HF + HNO3 + H2O etchDf - Hydride Formation
ML00175 — Localized External Wear of a Wire RopeM - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Highly strain hardened pearlitic structure of one external wire, 3.2mm diameter, of one strand.
55
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Pearlite
Micrographic detail of the strain hardened pearlitic structure, in a longitudinal section, of a 3.2mm external round wire of one strand. This structure presented a hardness level about 500 HV (1kg), measured in the center of the thickness in the metallographic section.
47
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Strain Hardened
Metallographic aspect of the wire surface in one strand external wire, showing the presence of oxides.
42
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - At the Surface
Metallographic detail of the wire surface in one strand external wire, showing the presence of oxides.
39
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Oxide Layer
Low magnification micrography of a strain hardened pearlitic structure, in a longitudinal section, of the 1.6mm round wire in the core.
34
VIEW
ML00175 / Aug.2021
Localized External Wear of a Wire Rope
M - High Carbon SteelP - Wire RopeAp - Oil and GasCd - Wear
Cm - Nital Etched Micrography by OMDf - Longitudinal Section

+4 more from this case →

ML00173 — Welding Cracks in an Aged HP Cast FittingM - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cast fitting microstructure. Network of primary carbides and austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Cast fitting microstructure. The material presented a network of primary carbided and an austenitic matrix with coalescing secondary precipitation.
37
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Micrographic detail of the network of primary carbided, white and grey, and an austenitic matrix with coalescing secondary precipitation.
30
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Aged Microstructure
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). The adopted filler metal is similar to the base metal.
27
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line
Fusion line between the aged base metal (in the top) and the weld metal (in the bottom). There is a region where the primary carbides melted (partially melted zone), that appears dark, and a region of high dilution cloe to the fusion line.
26
VIEW
ML00173 / May.2021
Welding Cracks in an Aged HP Cast Fitting
M - Heat Resistant SteelP - Cast FtittingAp - PetrochemicalCd - Welding
Cm - Kalling Etched Micrography by OMDf - Fusion Line

+5 more from this case →

ML00172 — Brittle Fracture of a LAS Valve SpringM - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Micrographic detail of the transverse section of the spring, at the surface, showing the pits full of corrosion deposits.
31
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Surface Deposits
Micrographic detail of spring surface, showing the pits full of corrosion deposits and a small decarburized layer (probably from the manufacturing processes).
30
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Decarburized Surface
Micrography of a longitudinal section of the spring, at the surface, indicating that there are multiple intergranular cracks initiating from the pit.
26
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Multiple cracks
Micrographic aspect of the multiple intergranular cracks, initiating from the bottom of a pit.
25
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Intergranular Cracking
Micrographic detail of the intergranular cracks, initiating from the bottom of a pit.
29
VIEW
ML00172 / Mar.2021
Brittle Fracture of a LAS Valve Spring
M - Low Alloy Medium Carbon QTP - SpringAp - Oil and GasCd - Brittle Fracture
Cm - As polished micrographyDf - Intergranular Cracking

+3 more from this case →

ML00171 — Corrosion Fatigue of U Bolt Pipe ClampM - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Metallographic detail of the longitudinal section of the clamp with a ferritic pearlitic structure.
32
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Metallographic detail of the ferritic perlitic structure.
31
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Metallographic aspect of a longitudinal section of the clamp, at the surface (left side of the image) showing a region where there are corrosion pits in the carbon steel clamp, due to the lack of protection by the coating, and the propagation of small transgranular cracks from to the surface.
30
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Micrography by OMDf - Crack
The clamp presented several cracks, parallel, transverse to the axis. The appearance of the cracks in the metallographic section shows that some cracks propagate and growth with a irregular path.
24
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Longitudinal Section
Metallographic aspect of the cracks showing that several microcracks join from different pits and growth through the section, in a transgranular morphologyy.
26
VIEW
ML00171 / Feb.2021
Corrosion Fatigue of U Bolt Pipe Clamp
M - Low Carbon SteelP - BoltAp - ShipCd - Corrosion Fatigue
Cm - Nital Etched Micrography by OMDf - Transgranular Cracking

+2 more from this case →

ML00170 — MIC in Aluminum Brass TubesM - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Micrographic detail of the granular structure of the aluminum brass, monophasic alpha.
44
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Alpha
Micrography of a transverse section of the tube, close to the leakage point. The thickness is localized reduced where the internal passive layer was ruptured, and the chemical effect of the biological proliferation created a high corrosion rate.
26
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Localized Thinning
Micrography of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
28
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
Micrographic detail of a transverse section of the tube at the localized reduced thickness point. Close to the internal surface.
26
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Internal Surface
MIC in Aluminum Brass Tubes
2
VIEW
ML00170 / Sep.2020
MIC in Aluminum Brass Tubes
M - Aluminum BrassP - Seamless tubeAp - MaritimeCd - Preferential Dissolution
Cm - FeCl3+HCl+Ethanol Etched MicroDf - Localized Corrosion

+1 more from this case →