Optical Microscope

47 cases · 467 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Standard: A clear all

Optical Microscope — sub-branches

As polished micrography 40Glyceregia Etched Micrography by OM 6Kalling Etched Micrography by OM 31Micrography by OM 23Micrography by OM using A262 Method A 43NaOH Electrolytic Etched Micro 52Nital Etched Micrography by OM 265Oxalic Acid Electrolytic Etch 7

Results

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Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure.
55
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrography of the longitudinal section, in the center of the thickness of the pin, presenting an aligned ferritic-austeinitic structure.
180
VIEW
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrography of the plate in a section, showing a ferritic-pearlitic microstructure in the middle of the thickness.
84
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the internal surface (left side). It is possible to see large graphite flakes.
98
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the Internal Surface
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
109
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Longitudinal section micrography in a position of the thread, far from the failure. The stud presented a quenching and tempering structure and the thread was machined.
84
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Machined Thread
Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
134
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface

More from these cases

ML00148 — Brittle Fracture of a 420 SS Barrel NutM - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Microstructural aspect of a longitudinal section of the nut, in the middle of the thickness. Martensitic structure, banded.
46
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Microstructural detail of the banded structure. The rough aspect of the band is created by the carbides (better seen in the higher magnification image) in the segregation band.
38
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Micrographic detail of the nut longitudinal section presenting the large carbides (white islands) in the segregation band, and small precipitates all through the martensite matrix, indicating that this high carbon steel was tempered in a high temperature. The 36HRc hardness also confirms this high tempering temperature.
39
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
Vickers microhardness identations using 100 grams. In a position out of the band (top line). Values from left to right, 380HV; 390HV and 394HV. In a position inside the band (bottom line). Values from left to right, 433HV, 483HV and 473 HV.
33
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure
Low magnification micrography of the nut in the longitudinal section, presenting the machined internal thread and a banded microstructure. It is possible to see that the contact pressure in the thread caused a surface plastically deformation.
24
VIEW
ML00148 / Sep.2018
Brittle Fracture of a 420 SS Barrel Nut
M - Martensitic Stainless SteelP - Barrel NutAp - LiftingCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Banded Structure

+6 more from this case →

ML00146 — Plastic Deformation of a SDSS Riser PinM - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Micrography of a longitudinal section, at the surface of the pin, where the thermal spray layer is sound. The thickness of the layer is about 0.3 mm.
168
VIEW
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Coating Layer
Micrographic detail of a longitudinal section of the pin, at the surface, evidencing the thermal spray layer, about 0.3 mm. The layer presents typical characteristics of multiple layers, low amount of entrapped oxides and pores. The interface presents a high roughness level for a good adherence and some entrapped oxides. The structure of the SDSS substrate did not show thermal effects.
154
VIEW
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Coating Layer
Micrography of a longitudinal section, at the damage surface of the pin, where the thermal spray layer was partially detached and broken. The through layer breaking is ductile, typical of an overloading condition caused by the localized bending of the pin.
109
VIEW
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Layer Detachment
Micrographic detail of the damage surface layer, detached and broken. The substrate is not affected and the rupture of the layer is typically by overloading.
117
VIEW
ML00146 / Jul.2018
Plastic Deformation of a SDSS Riser Pin
M - Super Duplex Stainless SteelP - PinAp - O&G Well DrillingCd - Bending
Cm - NaOH Electrolytic Etched MicroDf - Layer Detachment
ML00143 — Impact of a .308 Winchester on A36 PlateM - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Micrography of the plate in a section, showing a ferritic-pearlitic microstructure in the middle of the thickness, in a position where the plate was not affected by the shot.
65
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the plate in a section, showing a ferritic-pearlitic microstructure in the middle of the thickness.
66
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the ferritic-pearlitic microstructure.
53
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - Nital Etched Micrography by OMDf - Ferrite and Pearlite
Micrographic detail of the plate section, as polished, close to the surface that suffered the impact. The plate material deformed during the perforation,
31
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - As polished micrographyDf - Transverse Section
Micrographic detail of the plate section, as polished, close to the surface that suffered the impact. The copper alloy melted and created a yellow-orange deposit.
25
VIEW
ML00143 / Aug.2018
Impact of a .308 Winchester on A36 Plate
M - Low Carbon SteelP - Rolled PlateAp - StructureCd - Pierced
Cm - As polished micrographyDf - Melted film

+22 more from this case →

ML00141 — Brittle Fracture of a Corroded Gray Cast IronM - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), in the center of the thickness. It is possible to see a mixture of large graphite flakes and rosette grouping flakes.
80
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - In the Center of the Thickness
Micrographic aspect, as polished, of the cast cylinder section at the fracture position (top of the figure), close to the external surface (left side). It is possible to see smaller graphite flakes, interdendritic .
79
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the longitudinal section of the cylinder, at the internal diameter (left side of the figure), in contact with the treated cooling water, presenting large graphite flakes in a predominatly perlitic matrix.
50
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Close to the Internal Surface
Micrography of the longitudinal section of the cylinder, at the internal diameter, in contact with the treated cooling water, presenting large graphite flakes in a predominatly perlitic matrix. It is important to mention that the flakes are almost interconnecting themelves.
47
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Graphite in Flakes
Micrography of the longitudinal section of the cylinder, at the internal diameter, in contact with the treated cooling water, presenting large graphite flakes in a predominatly perlitic matrix. It is important to mention that the flakes are almost interconnecting themelves.
48
VIEW
ML00141 / Jul.2018
Brittle Fracture of a Corroded Gray Cast Iron
M - Gray Cast ironP - CastingAp - EngineCd - Brittle Fracture
Cm - Nital Etched Micrography by OMDf - Predominantly Pearlitic

+19 more from this case →

ML00138 — Liquid Metal Embrittlement of a HSLA SteelM - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Micrography of the high strenght steel, heat treated, of the casting device. The microstructure is bainitic martensitic.
92
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the high strenght steel microstructure, bainitic martensitic.
85
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainitic Martensitic
Micrographic detail of the zinc layer at the surface.
88
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer
Micrography of the section transverse to the fracture (top of the figure). The fracture is intergranular, there are several secondary cracks, and there are deposits of zinc over the fracture. The zinc makes difficult the etch with Nital to reveal the microstructure close to the fracture surface.
67
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture
Micrographic detail of the section transverse to the fracture (top of the figure), suggesting the intergranular morphology (at the previous austenite grain boundaries) and the deposits of zinc over the fracture that create a condition of protection of the base metal during the metallographic etch, and the material is not fully etched.
60
VIEW
ML00138 / Jun.2018
Liquid Metal Embrittlement of a HSLA Steel
M - High Strength Low AlloyP - Coated ProductAp - Mechanical IndustryCd - Liquid Metal Embrittlement
Cm - Nital Etched Micrography by OMDf - Zn Layer

+12 more from this case →

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Microstructure of the stud in the longitudinal section, presenting segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration.
69
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Microstructure of the stud in the longitudinal section, out of a region of segregation, where the tempered martensitic microstructure appears more uniform.
72
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic detail of the segregated bands, not uniformly distributed in the section. The bands are associated to elongated and aligned inclusions, and a refined microstructure, probably due to carbon and alloying elements concentration. The localized microhardness (50g) in the band showed levels about 540HV, and out of the band, in the same localtion, presented an average hardness of 321 HV, indicating that the material is non uniform in the regions where there are bands.
66
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
Micrographic detail of the martensitic structure of the stud in the longitudinal section, out of a region of segregation, where the microstructure appears more uniform and the microhardness is about 370HV (50g).
62
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Low magnification micrography of a stud longitudinal section in the first thread fillet adjacent to the fracture, presenting a large secondary crack without any deformation evidence. This reveals a brittle material behavior, although the hardness measured at the stud end revealed 33HRc, as should be expected by the material specification.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks

+17 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite

+8 more from this case →

ML00130 — Fatigue Fracture of Overloaded BoltsM - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section. The bolt was quenched and tempered to 30HRc and presented a martensitic structure.
124
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface
Micrographic detail of the rolled thread that was heat treated later. The bolt was quenched and tempered to 30 HRc and presented a martensitic structure.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
110
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - In the Center of the Thickness
The microstructure of the bolt is martensitic in the center of the thickness. Longitudinal section.
103
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - Martensite
Micrographic aspect of the rolled thread that was heat treated later. Longitudinal section.
115
VIEW
ML00130 / Jun.2018
Fatigue Fracture of Overloaded Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - O&G Well DrillingCd - Mechanical Fatigue
Cm - Nital Etched Micrography by OMDf - At the Surface

+3 more from this case →