Optical Microscope

110 cases · 389 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Damage Detail focus: Microstructure clear all

Optical Microscope — sub-branches

As polished micrography 9Chromic Acid Electrolytic Etched 1Eletrolytically Etched Micrography by OM 4FeCl3+HCl+Ethanol Etched Micro 6FeCl3+HCl+H2O Etched Micro 11Glyceregia Etched Micrography by OM 5H2SO4+HNO3+H3PO4 Etched Micro 2Kalling Etched Micrography by OM 44Keller Etched Micrography by OM 7Kroll Etched Micrography by OM 3Micrography by OM 14Micrography by OM using A262 Method A 25NaOH Electrolytic Etched Micro 34Nital Etched Micrography by OM 206Oxalic Acid Electrolytic Etch 18

Results

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Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the bainitic structure in the center of the pin, that was quenched and tempered after carburizing.
75
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Bainite
Micrographic detail of the quenched and tempered martensitic structure of the pin tool joint.
83
VIEW
ML00088 / Dec.2017
Hydrogen Cracking of an API 5D S135 Drill Pipe
M - Low Alloy Medium Carbon QTP - Drill PipeAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the link, presenting a tempered martensitic structure, typical of a quenching and tempering heat treatment and compatible with the link hardness of 43 HRc.
67
VIEW
ML00079 / Jul.2017
Hydrogen Cracking of a Maritime Chain Link
M - High Strength Low AlloyP - Chain LinkAp - OffshoreCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography of the bolt in the longitudinal section, showing a tempered martensitic structure, slightly banded.
97
VIEW
ML00077 / Jun.2018
Hydrogen Cracking of LAS Subsea Bolts
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Banded Structure
The stud presents an austenitic structure, with primary and secondary precipitates of a size that is visible in low magnification microscopy.
55
VIEW
ML00075 / Jun.2018
Hydrogen Cracking of IN 718 Subsea Fasteners
M - NiCrFe AlloyP - StudAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrographic aspect of the aged martensite structure of the 17-4 PH bolt, about 37 HRc.
94
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite
Tempered martensitic structure of a longitudinal section of the fastener. Slightly banded material. Hardness level about 42 HRc.
59
VIEW
ML00073 / Jun.2018
Hydrogen Cracking of a LAS Subsea Fastener
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite

More from these cases

ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
ML00081 — Hydrogen Cracking of a Chromium Plated Carburized PinM - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Micrography of a longitudinal section of the pin, at the surface. The pin was carburized, quenched and tempered (yellow diffuse layer at the surface, 0.5 mm of extension) and a white layer of hard chromium plating is evident.
108
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Carburized Layer
Micrographic detail of the high hardness martensitic structure at the surface of the pin, that was quenched and tempered after carburizing.
67
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Martensite
Micrography that presents a secondary cracking (adjacent to the broken surface) propagating 500 microns from the surface, where there is a white layer of hard chromium .
78
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Carburized Layer
The as polished micrography of a longitudinal section of the pin, showing several microcracks associated to the chromium layer.
56
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Hard Chromium Layer
The as polished micrography of a longitudinal section of the pin, showing that under the white layer of hard chromium (about 10 microns thick), there are already intergranular microcracks.
52
VIEW
ML00081 / Aug.2017
Hydrogen Cracking of a Chromium Plated Carburized Pin
M - Low Alloy for Thermochemical TreatmentP - Chromium PlatedAp - AutomotiveCd - Hydrogen Embrittlement
Cm - Micrography by OMDf - Hard Chromium Layer
ML00075 — Hydrogen Cracking of IN 718 Subsea FastenersM - NiCrFe AlloyP - StudAp - SubseaCd - Hydrogen Embrittlement
The stud structure evidences grain boundaries precipitation of probably delta phase (an overaging of the hardening precipitate).
49
VIEW
ML00075 / Jun.2018
Hydrogen Cracking of IN 718 Subsea Fasteners
M - NiCrFe AlloyP - StudAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00074 — Hydrogen Cracking of a 17-4 PH Subsea BoltM - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the aged martensite structure of the 17-4 PH bolt, about 37 HRc.
73
VIEW
ML00074 / Jun.2018
Hydrogen Cracking of a 17-4 PH Subsea Bolt
M - Precipitation Hardened Stainless SteelP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Martensite