Optical Microscope

3 cases · 34 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Standard: 182 clear all

Optical Microscope — sub-branches

Kalling Etched Micrography by OM 14NaOH Electrolytic Etched Micro 20

Results

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Microstructural analysis of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
106
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
74
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Base metal micrographic detail presenting a tempered martensitic microstructure.
27
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal

More from these cases

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic detail of the valve body structure, close to the position where the cracking has occurred. The structure is ferritic austenitic, with a large amount of detrimental phases associated to the ferritic structure, probably sigma phase.
102
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Metallographic detail of the large amount of sigma phase, associated to the ferritic structure.
105
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Sigma
Microstructural analysis of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
67
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
63
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the valve body structure, far from the position where the cracking has occurred, in the bottom of the body. The structure is ferritic austenitic, with some sigma phase, not in a large amount, indicating the valve structure was not uniform.
61
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite

+8 more from this case →

ML00123 — Non Qualified Superduplex for SubseaM - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. Coarse structure.
61
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrography of a transverse section of the forged bar in the center of the thickness. Ferrite and austenite. The ferrite amount, measured by metallographic method, manual counting, is 59%.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Transverse Section
Micrography of a longitudinal section of the forged bar in the center of the thickness. Ferrite and austenite. The average austenite spacing is 80 microns, a lot larger than the maximum allowed in the specification, of 30 microns. No detrimental phases were identified at the ferrite/austenite interfaces, but the ferrite phase presented a rough aspect. Higher magnification analysis would be required to identify precipitation.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Longitudinal Section
Micrographic detail of the ferrite and austenite structure in the transverse section of the forged bar, in the center of the thickness.
53
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
Micrographic detail of the ferrite and austenite structure in the longitudinal section of the forged bar, in the center of the thickness.
55
VIEW
ML00123 / Feb.2018
Non Qualified Superduplex for Subsea
M - Super Duplex Stainless SteelP - BarAp - Oil and GasCd - Not according to spec
Cm - NaOH Electrolytic Etched MicroDf - Ferrite and Austenite
ML00045 — Subsea Tubular F6NM Martensitic SSM - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Micrographic detail of the heat-affected zone close to the base metal.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the heat-affected zone close to the fusion line.
31
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone
Micrographic detail of the tempered martesite weld metal close to the fusion line. The columnar grains can be observed .
22
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Weld Metal
Micrography of the base metal showing a tempered martensitic microstructure.
29
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Base Metal
Micrography of the heat-affected zone. The fusion line is in the right and the coarse structure of the base metal is refined at the heat affected zone.
28
VIEW
ML00045 / Aug.2017
Subsea Tubular F6NM Martensitic SS
M - Martensitic Stainless SteelP - Fabrication WeldAp - OffshoreCd - Welding
Cm - Kalling Etched Micrography by OMDf - Heat Affected Zone

+8 more from this case →