Optical Microscope

16 cases · 78 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Subsea Detail focus: Damage clear all

Optical Microscope — sub-branches

As polished micrography 12Kalling Etched Micrography by OM 23Micrography by OM 5Micrography by OM using A262 Method A 6NaOH Electrolytic Etched Micro 4Nital Etched Micrography by OM 28

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Micrography of a longitudinal section of the bolt, in a position close to the fracture (top) and bolt surface (left ), presenting several secondary intergranular cracks.
57
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Intergranular Cracking
Low magnification micrography of a stud longitudinal section in the first thread fillet adjacent to the fracture, presenting a large secondary crack without any deformation evidence. This reveals a brittle material behavior, although the hardness measured at the stud end revealed 33HRc, as should be expected by the material specification.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks
Low magnification micrographic aspect of the cracking. It is brittle, transgranular and associated to the ferritic/sigma phase interfaces.
54
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Brittle Cracks
Micrography of the longitudinal section of the bolt, at the fracture (top of the figure), starting from the bottom of the thread (to the left side of the figure). The presence of the coating at the bolt surface shows that the fracture occurred without corrosion. The rusted aspect of the fracture is associated to corrosion products after the rupture has occurred, also suggesting that the bolts were fractured and remained in service for some time after the failure occurred.
65
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Fracture
Micrographic detail of the crevice corrosion in the case wall, showing that the structure is not affected and is fully austenitic with equiaxial grains typical of a solution annealed condition.
85
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
17-4 PH rod. Micrography of the longitudinal section close to the surface, presenting the roughness (the waves at the surface) and a region where a pitting was still in the beginning, not related to any specific microstructure.
70
VIEW
ML00121 / Feb.2018
Pitting Corrosion in a Subsea System
M - Austenitic / MartensiticP - Rod & CylinderAp - SubseaCd - Pitting Corrosion
Cm - Kalling Etched Micrography by OMDf - Pitting
Micrographic detail of the region where the cracking was initiated at the internal side of the fitting.
41
VIEW
ML00094 / Sep.2017
MIC of a Subsea Hydraulic Line
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Behavior
Cm - NaOH Electrolytic Etched MicroDf - Through Wall Cracking
The disc spring presented several small pits, as this one, that did not propagate.
24
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Nital Etched Micrography by OMDf - Pitting

More from these cases

ML00139 — Hydrogen Fracture of a 17-4 PH Allen BoltM - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Micrographic detail of the secondary intergranular cracks close to the surface of the bolt, where the fracture occurred.
56
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Intergranular Cracking
Micrography of a longitudinal section of the bolt, close to the fracture surface (top of the figure). The fracture is macroscopically flat and started at the surface (left side) in a position close to the bolt body to bolt head transition. The structure is aged martensite.
55
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Brittle Fracture
Micrography of a longitudinal section of the bolt, in a position close to the fracture (top) and bolt surface (left ), presenting several secondary intergranular cracks. The structure is aged martensite and the cracks are located in the previous austenite grain boundaries.
52
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Fracture
Micrographic detail of the secondary intergranular cracks (in the previous austenite grain boundaries).
49
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks
Micrographic detail of the secondary intergranular cracks (in the previous austenite grain boundaries).
48
VIEW
ML00139 / Jun.2018
Hydrogen Fracture of a 17-4 PH Allen Bolt
M - Precipitation Hardened Stainless SteelP - Allen BoltAp - SubseaCd - Hydrogen Embrittlement
Cm - Kalling Etched Micrography by OMDf - Secondary Cracks

+7 more from this case →

ML00136 — Hydrogen Cracks of Subsea StudsM - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Low magnification micrography showing how the large secondary crack propagated in the thickness of the stud, with a branching aspect, different than the propagation close to the bottom of the thread fillet.
47
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks
Low magnification micrography of the bottom of the thread fillet, presenting secondary cracks, not yet opened.
44
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks
Low magnification micrography of another thread fillet, presenting secondary cracks from the bottom of the thread, not yet opened.
45
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Crack
As polished micrography of the bottom of the thread fillet, where a cracking is still closed, showing the microscopical morphology of the cracking.
40
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Cracking
As polished micrographical detail of the cracks at the bottom of the thread fillet. There are several small cracks some of them associated to longitudinal inclusions. There are some regions presenting small "pores".
40
VIEW
ML00136 / Jun.2018
Hydrogen Cracks of Subsea Studs
M - Low Alloy Medium Carbon QTP - FastenerAp - SubseaCd - Hydrogen Embrittlement
Cm - As polished micrographyDf - Crack

+12 more from this case →

ML00134 — Brittle Fracture of a Superduplex Valve BodyM - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Micrographic details of the cracking. It is brittle, transgranular and associated to the ferritic/sigma phase interfaces.
50
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Brittle Cracks
Micrographic aspect of the cracking. It is brittle, transgranular and associated to the ferritic/sigma phase interfaces.
49
VIEW
ML00134 / Aug.2020
Brittle Fracture of a Superduplex Valve Body
M - Super Duplex Stainless SteelP - Fabrication WeldAp - SubseaCd - Brittle Fracture
Cm - NaOH Electrolytic Etched MicroDf - Brittle Cracks
ML00126 — Hydrogen Fracture of Subsea Allen BoltsM - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Micrography, after NItal etching, of the longitudinal section of the bolt, at the fracture (top of the figure), starting from the bottom of the thread (to the left side of the figure). The presence of the coating at the bolt surface shows that the fracture occurred without corrosion.
56
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Fracture
Micrography of the longitudinal section of the bolt, in the center of the thickness, showing at the fracture surface (top of the figure), secondary cracks that are perpendicular to the fracture, associated to segregation bands.
55
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks
Micrographic detail of the longitudinal section of the bolt, in the center of the thickness, showing the secondary cracks associated to segregation bands.
63
VIEW
ML00126 / Mar.2018
Hydrogen Fracture of Subsea Allen Bolts
M - Low Alloy Medium Carbon QTP - Coated ProductAp - SubseaCd - Hydrogen Embrittlement
Cm - Nital Etched Micrography by OMDf - Secondary Cracks
ML00122 — Crevice Corrosion in a Subsea SystemM - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Micrographic detail of the crevice corrosion in the case wall, showing that the structure is not affected and is fully austenitic with equiaxial grains typical of a solution annealed condition.
72
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
Micrographic detail of the crevice corrosion in the case wall, showing that the structure is not affected and is fully austenitic with equiaxial grains typical of a solution annealed condition. Even non metallic inclusions did not accelerate corrosion since the extension of the inclusions was not too long and they were not connecting to others.
76
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
Micrographic detail of the crevice corrosion in the case wall, showing that the structure is not affected and is fully austenitic with equiaxial grains typical of a solution annealed condition. Even non metallic inclusions did not accelerate corrosion since the extension of the inclusions was not too long and they were not connecting to others.
81
VIEW
ML00122 / Feb.2018
Crevice Corrosion in a Subsea System
M - Austenitic Stainless SteelP - CaseAp - Oil and GasCd - Crevice
Cm - Micrography by OM using A262 Method ADf - Localized Corrosion
ML00080 — MIC of Stacking Disc SpringsM - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Micrographic aspect of the disc fracture (in the right side of the figure). It is possible to see that the structure is martensitic and there are secondary intergranular cracks associated to the fracture.
25
VIEW
ML00080 / Sep.2017
MIC of Stacking Disc Springs
M - Low Alloy Medium Carbon QTP - SpringAp - SubseaCd - Brittle Behavior
Cm - Nital Etched Micrography by OMDf - Intergranular Cracking