Optical Microscope

7 cases · 67 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Application: Chemical Industry Detail focus: Sampling and Analysis clear all

Optical Microscope — sub-branches

As polished micrography 5Kalling Etched Micrography by OM 16Keller Etched Micrography by OM 12Kroll Etched Micrography by OM 7Micrography by OM 5Micrography by OM using A262 Method A 14NaOH Electrolytic Etched Micro 2Oxalic Acid Electrolytic Etch 6

Results

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Low magnification micrography transverse to the fillet weld in the pipe. The pipe base metal is to the bottom of the figure and the weld metal is to the top. The heat affected zone in the middle, shows a coarse grain size structure.
59
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Welded Joint
The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
SAMPLE 1 AT THE FRACTURE - Micrography in low magnification where the thickness is reduced to zero (fracture). Side A (process side) to the bottom and side B (furnace environment side) to the top.
85
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
Micrography of the pipe longitudinal base metal.
148
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Micrography of a longitudinal section of the pipe AA 3003. Granular structure that reveals the forming direction and dispersed particles.
229
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrography of a longitudinal section of the fitting, at the base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
44
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
The micrography of the welded joint between the flange and the shell, in a region that was through wall cracked, the fracture propagating in the shell plate base metal.
74
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Welded Joint

More from these cases

ML00179 — Hydrides in Titanium WeldM - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Low magnification micrography showing the weld metal, full of pores, indicating that the field welding was not properly shileded.
50
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Coarse grains in the heat affected zone.
46
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone
Micrography of the weld metal at the fillet weld where the cracking started, showing several brittle microcracks that corresponds to the regions where the fractography showed secondary crackis.
35
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Micrographic detail of the weld metal brittle microcracks, in regions with hydrides formation.
32
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Weld Metal
Brittle crack in the surface of the welded joint, at the heat affected zone close to the fusion line.
30
VIEW
ML00179 / Feb.2022
Hydrides in Titanium Weld
M - Unalloyed TitaniumP - In Field WeldAp - Chemical IndustryCd - Hydride Formation
Cm - Kroll Etched Micrography by OMDf - Heat Affected Zone

+6 more from this case →

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Micrography of the stub end, external side to the top, presenting multiple cracks propagating throught wall.
48
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - As polished micrographyDf - Close to the External Surface
Micrography of the stub end close to the external surface, outer diameter in the top of the image, presenting multiple cracks starting fro the surface and propagating into the thickness, through wall.
32
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Close to the External Surface
Micrography of the stub end in the middle of the thickness, outer diameter to the top of the image, presenting multiple branched cracks.
27
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - In the Center of the Thickness
ML00160 — High Temperature Degradation of 310SSM - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
SAMPLE 1 AT 1 mm THICKNESS - Micrography in low magnification in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation.
77
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 2 AT 2 mm THICKNESS - Micrography in low magnification in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation. No variation in the microstructure of the center of the plate, compared to sample 1.
52
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - Oxalic Acid Electrolytic EtchDf - Low Mag
SAMPLE 3 AT 4 mm THICKNESS - Micrography in low magnification in the center of the thickness. The microstructure is austenitic with secondary intergranular and intragranular precipitation, but this micrography was obtained in the longitudinal section, presenting the plate alignment and was etched with NaOH, adopted to colour the sigma phase .
40
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - NaOH Electrolytic Etched MicroDf - Low Mag
SAMPLE 1 AT 1 mm THICKNESS - Micrography in low magnification in the center of the thickness, as polished. There are no regions of internal damage (like internal voids or cracks), indicating that the mechanism is only related to surface effects.
42
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - In the Center of the Thickness
SAMPLE 3, CLOSE TO THE SURFACE OF SIDE A - Micrography, as polished, of the oxides at the process side. In this region there is an oxide layer, not continuous but with no localized penetrations.
43
VIEW
ML00160 / Apr.2020
High Temperature Degradation of 310SS
M - Austenitic Stainless SteelP - Rectangular TubeAp - Chemical IndustryCd - Scaling
Cm - As polished micrographyDf - At the Surface

+3 more from this case →

ML00065 — Erosion Corrosion of Monel PipingM - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Micrographic detail of the pipe base metal presenting a granular microstructure. Some inclusions are also visible.
142
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Left Side
Micrography of the elbow base metal. The comparison with the pipe micrography shows an important difference of thickness.
132
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Elbow base metal micrographic detail presenting a granular microstructure. Like the pipe, the microstructure reveals inclusions.
106
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Base Metal Right Side
Micrography of the pipe heat affected zone. The weld metal is on the right.
91
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side
Micrographic detail of the pipe fusion line. The pipe heat affected zone is at the bottom and the weld metal is at the top.
86
VIEW
ML00065 / May.2017
Erosion Corrosion of Monel Piping
M - NiCu AlloyP - Seamless PipeAp - Chemical IndustryCd - Erosion Corrosion
Cm - Kalling Etched Micrography by OMDf - Fusion Line Left Side

+10 more from this case →

ML00059 — Intergranular Corrosion of Aluminum PipingM - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Micrographic detail of a longitudinal section of the pipe AA 3003. Granular structure and dispersed particles.
199
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Left Side
Micrography of a longitudinal section of the pipe AA 6063. Granular structure and dispersed particles.
169
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Base Metal Right Side
Micrography of the Fusion Line of the AA 3003 pipe, presenting a narrow HAZ.
127
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Fusion Line Left Side
Micrography of the Fusion Line of the AA 3003 pipe, presenting a narrow HAZ.
110
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Fusion Line Left Side
Micrographic detail of the Fusion Line of the AA 3003 pipe, presenting a narrow HAZ.
93
VIEW
ML00059 / Feb.2018
Intergranular Corrosion of Aluminum Piping
M - Aluminum ManganeseP - Welded JointAp - Chemical IndustryCd - Intergranular Corrosion
Cm - Keller Etched Micrography by OMDf - Fusion Line Left Side

+6 more from this case →

ML00061 — Creep in a Seam Weld of a 304H SS FittingM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Micrographic detail of the fitting base metal, presenting an austenitic structure with intergranular and transgranular precipitation as a result of microstructural evolution.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Base Metal
Micrography of a transverse section of the seam weld, close to the internal surface, presenting several cracks perpendicular to the thickness.
37
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Close to the Internal Surface
Micrographic detail of the seam weld close to the internal surface, presenting the needles that are the result of microsctructural evolution and cracks filled with oxides.
36
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - Close to the Internal Surface
Micrography of a transverse section of the seam weld, in the middle of the thickness, presenting several parallel cracks.
27
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - In the Center of the Thickness
Micrographic detail of the seam weld in the middle of the thickness, presenting the needles that are the result of microsctructural evolution and cracks filled with oxides.
40
VIEW
ML00061 / Apr.2017
Creep in a Seam Weld of a 304H SS Fitting
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Creep
Cm - Micrography by OM using A262 Method ADf - In the Center of the Thickness

+6 more from this case →

ML00050 — Fatigue Failure of a 316SS Pressure StabilizerM - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
The micrography of the welded joint between the flange and the shell, in a region that was not yet macroscopically cracked, presented a fatigue crack from the margin of the fillet weld.
72
VIEW
ML00050 / Nov.2017
Fatigue Failure of a 316SS Pressure Stabilizer
M - Austenitic Stainless SteelP - Fabrication WeldAp - Chemical IndustryCd - Mechanical Fatigue
Cm - Micrography by OM using A262 Method ADf - Welded Joint