Oxalic Acid Electrolytic Etch

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Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrography of a longitudinal section, in the center of the valve body, solid 3" thickness. The structure is austenitic with delta ferrite in interdendritic spaces.
67
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

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ML00164 — Austenitic SS Casting for Valve BodyM - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Micrography of a longitudinal section, in the center of the valve body. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite presents a cored matrix in the dendrites, indicating the chemical composition was not homogeneized during the heat treatment.
60
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the cored austenitic structure with delta ferrite in interdendritic spaces. The chemical composition was not homogeneized during the heat treatment.
55
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrography of a longitudinal section, in the 1" thickness valve wall. The structure is austenitic with delta ferrite in interdendritic spaces.
48
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of a longitudinal section, in the valve wall 1" thick. The structure is austenitic with delta ferrite in interdendritic spaces. The austenite is clean indicating that the homogeneization of a smaller thickness in the heat treatment is considered effective.
40
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
Micrographic detail of the clean austenitic matrix, with delta ferrite in interdendritic spaces.
35
VIEW
ML00164 / Jun.2020
Austenitic SS Casting for Valve Body
M - Austenitic Stainless SteelP - CastingAp - ValveCd - Typical manufacturing
Cm - Oxalic Acid Electrolytic EtchDf - Delta ferrite
ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Detailed aspect of the stress corrosion cracks in a longitudinal section of the fractured bolt, under the thread. The microstructure is strain hardened austenite.
47
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

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