Oxalic Acid Electrolytic Etch

3 cases · 27 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

Condition: Corrosion clear all

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The stub end was manufactured from a plate and the microstructure in a longitudial section shows a refined granular austenitic structure.
62
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were almost removed by the stress corrosion cracks.
756
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
76
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section

More from these cases

ML00168 — SCC of Austenitic SS Flange Stub EndM - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Micrography of a longitudinal section of the stub end showing a refined austenitic structure.
57
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrographic detail of the austenitic structure. Free from grain boundaries carbide precipitation.
53
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Micrography of the stub end close to the external surface, outer diameter in the top of the image, presenting multiple cracks starting fro the surface and propagating into the thickness, through wall.
32
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Close to the External Surface
Micrography of the stub end in the middle of the thickness, outer diameter to the top of the image, presenting multiple branched cracks.
27
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - In the Center of the Thickness
Micrography of the stub end longitudinal section, showing multiple branched transgranular cracks.
25
VIEW
ML00168 / Aug.2020
SCC of Austenitic SS Flange Stub End
M - Austenitic Stainless SteelP - Stub EndAp - Chemical IndustryCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transgranular Cracking

+2 more from this case →

ML00157 — Bolts Under Chloride SCC ConditionsM - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Low magnification micrography, by optical microscope, of the longitudinal section of a damaged bolt, in the center of the thickness. The microstructure is austenitic, free from carbides.
100
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Detail of the strain hardened austenitic microstructure. Micrography by optical microscope, of the longitudinal section of a bolt, in the center of the thickness.
76
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Strain Hardened
Optical micrography of a longitudinal section of the fractured bolt, at the thread. The material is austenitic, free from carbides, and the threads were fully cracked by the stress corrosion mechanism.
58
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Optical micrography of a longitudinal section of the fractured bolt, under the thread, showing stress corrosion cracks through the section.
46
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks
Detailed aspect of the stress corrosion cracks in a longitudinal section of the fractured bolt, under the thread. The microstructure is strain hardened austenite.
47
VIEW
ML00157 / Feb.2020
Bolts Under Chloride SCC Conditions
M - Austenitic Stainless SteelP - BoltAp - Oil and GasCd - Stress Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Stress Corrosion Cracks

+1 more from this case →

ML00135 — MIC of a Non Magnetic Drilling ToolM - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Optical micrography of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
64
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Transverse Section
Micrographic detail of the transverse section of the drill collar, in the center of the thickness, presenting an uniform, granular, fully austenitic microstructure.
61
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked. The material presented 38HRc hardness.
57
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Optical micrography of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked.
62
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Longitudinal Section
Micrographic detail of the longitudinal section of the drill collar, in the center of the thickness, presenting slightly elongated grains of fully austenitic microstructure, cold worked.
59
VIEW
ML00135 / May.2018
MIC of a Non Magnetic Drilling Tool
M - High Mn Austenitic SteelP - Tubular ForgingAp - O&G Well DrillingCd - Pitting Corrosion
Cm - Oxalic Acid Electrolytic EtchDf - Austenite

+6 more from this case →