Kalling Etched Micrography by OM

9 cases · 30 images

Crevice Corrosion in a Subsea System — Aspect Before Analysis

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Micrography of a transverse section of the ring presenting a uniform tempered martensite structure.
43
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
Micrography of a longitudinal section of the pin, presenting a tempered martensitic structure with aligned delta ferrite and carbide phases.
80
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the austenitic structure at the surface, where the grain size of the material increased. By optical microscopy the intragranular precipitation due to solution annealing and aging is not revealed.
794
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
Micrography of the nut in the longitudinal direction, at the Nylon insert position, showing a cold formed region at the end of the nut, with high hardness levels (about 600 HV100g).
53
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened
Granular austenitic structure close to the surface of the shaft.
61
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Austenite
13Cr SS in the longitudinal section, at the collapsed region. Detail of the non uniform structure (ferritic matrix and decorated prior austenite grain boundaries) that evidences an usuitable heat treatment during fabrication, and explains the material low strenght.
48
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Prior Austenite Boundaries Decorated
Blade microstructure. Tempered martensite, (probably) retained austenite and delta ferrite islands.
55
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Delta Ferrite Islands
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
114
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite

More from these cases

ML00124 — MIC of a Martensitic Valve RingM - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Micrography of a transverse section of the ring at the cracking position. The cracks are intergranular and opened at the position close to the surface.
27
VIEW
ML00124 / Feb.2018
MIC of a Martensitic Valve Ring
M - Martensitic Stainless SteelP - ForgingAp - EnergyCd - Brittle Behavior
Cm - Kalling Etched Micrography by OMDf - Martensite
ML00046 — Brittle Fracture of SS Shear PinM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Micrographic detail of the pin structure, in the longitudinal section, at the segregated band with aligned inclusions and phases, delta ferrite and carbides.
70
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
Micrographic detail of the pin structure, in the longitudinal section, presenting a martensitic matriz, aligned inclusions (grey, delta ferrite islands (poligonal white phases) and carbides (also white phases) surrounding the delta ferrite.
64
VIEW
ML00046 / Jan.2018
Brittle Fracture of SS Shear Pin
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Intergranular Cracking
Cm - Kalling Etched Micrography by OMDf - Martensite, delta ferrite & carbides
ML00089 — Inconel 718 Allen Bolt for Subsea ApplicationM - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
The micrography of a longitudinal section of the bolt, in the center of the thickness (ND 1/2"), shows an equiaxial granular structure. Although the material was hardened by heat treatment (solution annealing and aging), the microstructure at this magnification does not reveal the intragranular precipitation.
34
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Equiaxial Grains
Micrographic detail of a longitudinal section of the bolt, close to the surface (ND 1/2"). The grain size is higher than the center of the bolt.
28
VIEW
ML00089 / Sep.2017
Inconel 718 Allen Bolt for Subsea Application
M - NiCrFe AlloyP - Machined PartAp - SubseaCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Austenite
ML00062 — Inconel 718 Lock Nut with Polymer InsertM - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Micrographic detail of the nut at the cold formed region where the nut was bent over the Nylon insert. It is possible to see strain hardened structures (600HV 100g).
41
VIEW
ML00062 / Apr.2017
Inconel 718 Lock Nut with Polymer Insert
M - NiCrFe AlloyP - Cold FormedAp - PipingCd - Typical manufacturing
Cm - Kalling Etched Micrography by OMDf - Strain Hardened
ML00041 — Fatigue Fracture of Inconel 718 Spline ShaftM - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Duplex grain size structure, austenitic. The small grains are probably due to the arresting effect of the delta phase during fabrication in high temperature.
47
VIEW
ML00041 / Jun.2017
Fatigue Fracture of Inconel 718 Spline Shaft
M - NiCrFe AlloyP - ShaftAp - Oil and GasCd - Vibration Induced Fatigue
Cm - Kalling Etched Micrography by OMDf - Duplex structure
ML00039 — Collapse in Tubular 13CrM - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
The micrography of the 13Cr SS in the transverse section, at the collapsed region, shows a ferritic matrix structure (overtempered) with the previous austenite grain boundaries decorated by phases (carbides and probably martensite islands), indicating that the material was exposed to a high tempering temperature that created a partial austenitizing condition. It explains the material low toughness and lower strenght (than required).
32
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Overtempered Structure
The micrography of the 13Cr SS in the transverse section, far from the collapsed region, shows a uniform tempered martensitic structure.
32
VIEW
ML00039 / Apr.2017
Collapse in Tubular 13Cr
M - Martensitic Stainless SteelP - Seamless PipeAp - Oil and GasCd - Heat Treatment Defect
Cm - Kalling Etched Micrography by OMDf - Martensite
ML00017 — Casting Defect in CA6NMM - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Blade microstructure. Previous austenite coarse grains.
47
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Coarse Structure
Blade microstructure. Tempered martensite, (probably) retained austenite and delta ferrite islands.
48
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Delta Ferrite Islands
Blade structure close to the region where the voids were detected.
41
VIEW
ML00017 / Apr.2017
Casting Defect in CA6NM
M - Martensitic Stainless SteelP - Machined PartAp - EnergyCd - Casting Defect
Cm - Kalling Etched Micrography by OMDf - Non Metallic Inclusions
ML00011 — Intergranular SCC of Pure NickelM - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
110
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite
Microstructure of the fitting in the transverse section, presenting a granular Ni austenitic structure. No evidences of any phase in the grain boundaries.
96
VIEW
ML00011 / Oct.2017
Intergranular SCC of Pure Nickel
M - Unalloyed NickelP - Wrought FittingAp - Chemical IndustryCd - Stress Corrosion
Cm - Kalling Etched Micrography by OMDf - Austenite